摘要
用０．０５ｍｏｌ三氯硫磷和０．１０ｍｏｌ的酚通过相转移催化反应合成Ｏ，Ｏ-二芳氧基硫代磷酸氯可得较好收率。产物经ＩＲ和１ＨＮＭＲ表征。
Diaryl chlorothiophosphates have been prepared in a good yield from thiophosphoryl chlorideand two equivalents of a respective phenol by a phase-transfer-catulyzed proceSs. The products were charac- terized by IR and 1H NMR.
出处
《合成化学》
CAS
CSCD
1999年第1期4-5,共2页
Chinese Journal of Synthetic Chemistry
关键词
二芳基
硫代
磷酰氯
相转移催化
合成
Thiophosphoryl chloride, Phenol, O,O-diphenyl chlorothiophosphate, Synthesis, Phasetransfer-tatalyzed.
