摘要
目的:建立消脂护肝片中总黄酮的含量测定方法。方法:采用分光光度法,以芦丁为对照品,对其进行络合显色,在510nm波长处测定吸光度,从而测定消脂护肝片中总黄酮的含量。结果:线性范围在0.008~0.08mg.mL-1(r=0.9997),平均回收率为97.0%,RSD=1.84%(n=6)。结论:该法简便易行、重现性好、结果可靠,可用于该制剂的质量控制。
Objective: To establish ultraviolet sepctrophotometry for the determination of total flavones in Xiaozhihugan tablets. Methods: Quercetin was selected as reference material,and the samples were determined at 510 nm. Results: The linear range for quercetin was 0. 008 - 0. 08 mg· mL^-1 ( r = 0. 999 7 ). The recovery rate was 97.0 %, RSD = 1.84 % (n = 6) . Conclusion: This method is easy to handle with good accuracy and reproducibility, and is suitable for the quality control of Xiaozhihugan tablets.
出处
《中国现代中药》
CAS
2010年第10期31-32,37,共3页
Modern Chinese Medicine
关键词
消脂护肝片
总黄酮
分光光度法
Xiaozhihugan tablets
Total Flavones
Sepctrophotometry