摘要
运用气相色谱-离子阱串联质谱对烟草中20种有机磷农药残留分析条件进行研究,并分别通过全扫描、单极质谱选择离子(SIM)和二级质谱(MS/MS)3种模式比较其效果.结果显示,全扫描模式不能将20种有机磷农药的峰完全分离,而MS/MS和SIM模式在定性、定量上各具优势,因此在做样品分析时可同时通过两者进行检测,以达到最佳分析条件.
Analytical conditions of organophosphorous pesticide residues in tobacco are studied by ion-trap GC/MS/MS. Organophosphorous pesticide residues are separately detected by full scan mode, selected ion mode（SIM） and MS/MS mode. The results show that twenty peaks of organ- ophosphorous pesticides could not be separated completely in full scan mode. However, SIM and MS/MS mode have their own respective advantage on qualification and quantification, thus samples could be analyzed by both at the same time in order to achieve the best analytical conditions.
出处
《郑州大学学报（理学版）》
CAS
北大核心
2010年第4期75-79,共5页
Journal of Zhengzhou University:Natural Science Edition
基金
国家自然科学基金资助项目
编号J0830412
