摘要
以冰片、薄荷醇和2-四氢呋喃甲酸为原料,在纳米固体超强酸S2O28-/ZrO2的催化下合成了2-四氢呋喃甲酸冰片酯和2-四氢呋喃甲酸薄荷酯,酯化率分别为67.6%和53.8%,其结构经NMR,IR和元素分析表征。
2-Tetrahydrofuroic acid borneol ester and 2-tetrahydrofuroic acid menthol ester were synthesized by the reaction of 2-tetrahydrofuroic acid with borneol or menthol using solid superacid S2O2-8/ZrO2 as the catalyst.The yield of easter were 67.6% and 53.8%,respectively.The structures were characterized by NMR,IR and elemental analysis.
出处
《合成化学》
CAS
CSCD
北大核心
2010年第6期754-755,759,共3页
Chinese Journal of Synthetic Chemistry
基金
"重大新药创制"科技重大专项基金资助项目(2009ZX09103-121)
关键词
纳米固体超强酸
冰片酯
薄荷酯
催化合成
nanometer solid superacid
borneol ester
menthol ester
catalytic synthesis
