摘要
在微波辅助、无溶剂、无催化剂条件下,以取代吡唑甲醛,2-氨基苯并噻唑和亚磷酸二乙酯为原料,"一锅煮"合成了6个新型含吡唑与苯并噻唑环的α-氨基膦酸酯衍生物,其结构经1H NMR,13C NMR和MS表征。
A series of novel α-aminophosphonates derivatives containing pyrazole and benzothiazole were synthesized from substituted pyrazole aldehyde,2-aminobenzothiazole and diethylphosphone under microwave-assisted without catalyst and solvent.The structures were characterized by 1H NMR,13C NMR and MS.
出处
《合成化学》
CAS
CSCD
北大核心
2011年第1期78-80,84,共4页
Chinese Journal of Synthetic Chemistry
基金
河南省高校科技创新团队支持计划资助项目(2008IRTSTHN002)
关键词
Α-氨基膦酸酯
吡唑
苯并噻唑
微波无溶剂合成
α-aminophosphonates
pyrazole
benzothiazole
microwave-assisted solvent-free synthesis
