摘要
以对羟基苯甲酸、3-溴丙烯、3,3′,5,5′-四甲基联苯二酚等为原料,通过间氯代过氧化苯甲酸氧化法合成4,4′-双（4-羟基苯甲氧基）3,3′,5,5′-四甲基联苯二缩水甘油醚,化合物结构用FT-IR和~1HNMR进行了表征。并对氢氧化钠用量,缚酸剂,氧化反应温度和时间的选择进行了讨论。
4,4＇-bis（4-hydroxybenzoyloxy）-3,3＇,5,5＇-tetramethylbiphenyl was synthesized from p-hydroxybenzoic acid,3-bromopropene and 3,3＇,5,5＇-tetramethyl-diphenol,using m-choroperoxybenzoic acid as oxidant,and the structure of the synthesized product was characterized by means of IR and ~1HNMR.The effects of the amount of base,deacid reagent,the reaction temperature and time on the yield of the product were investigated.
出处
《精细与专用化学品》
CAS
2011年第6期23-25,共3页
Fine and Specialty Chemicals
基金
甘肃省科技厅"科技支撑计划"(0804GKCA019)
