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N-1-(1-金刚烷基)苯并三氮唑的简便合成及其结构表征

N-1-(1-adamantanyl) benzotriazole Synthesis and Structural Characterization
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摘要 由1-金刚烷醇与苯并三氮唑在浓硫酸介质下,室温搅拌2 h合成N-1-(1-金刚烷基)苯并三氮唑,产率为95%;产物结构经IR,1H NMR,13C NMR以及NOE等手段进行表征;该合成方法具有简便快速、产率高等优点。 By the 1-adamantanol and benzotriazole in sulfuric acid medium,stirring 2 h at room temperature,N-1-(1-adamantanyl) benzotriazole was synthesized with the yield of 95%.The product structure by IR,1H NMR,13C NMR and NOE were characterized.This method was simple,rapid,high yield,etc.
出处 《广州化工》 CAS 2011年第21期52-53,共2页 GuangZhou Chemical Industry
基金 浙江省分析测试科技计划项目(2011C37051) 浙江省教育厅科研项目(Y200805661)
关键词 1-金刚烷醇 N-1-(1-金刚烷基)苯并三氮唑 合成 结构表征 1-adamantanol synthesis N-1-(1-adamantanyl) benzotriazole characterization
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参考文献8

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