摘要
目的:对栾树花进行化学成分研究。方法:采用硅胶、聚酰胺柱层析进行分离纯化,根据理化性质和光谱分析鉴定化合物结构。结果:从栾树花乙酸乙酯部位中分离得到9个化合物,经鉴定分别为:胡萝卜苷(Ⅰ)、没食子酸(Ⅱ)、山柰酚(Ⅲ)、木犀草素(Ⅳ)、山柰素-3-O-(6″-乙酰基)-β-D-葡萄糖苷(Ⅴ)、2″-O-乙酰基金丝桃苷(Ⅵ)、2″-O-没食子酰基金丝桃苷(Ⅶ)、金丝桃苷(Ⅷ)、山柰酚-3-O-β-D-葡萄糖苷(Ⅸ)。结论:9个化合物均为首次从栾树花中分离得到;化合物Ⅳ、Ⅴ、Ⅵ和Ⅸ为首次从该属植物中分离得到。
Objective：To study the chemical constituents from flowers of Koelreuteria paniculata.Methods：Column chromatography and spectral analysis were used to isolate and identify the constituents.Results： The EtOAc fraction from flowers of Koelreuteria paniculata was separated and purified.Nine compounds were obtained and identified as：sitosterol glucoside（Ⅰ）,gallic acid（Ⅱ）,kaempferol（Ⅲ）,luteolin（Ⅳ）,kaempferol-3-O-（6″-acetyl）-β-D-glucopyranoside（Ⅴ）,hyperoside-2″-O-acetyl（Ⅵ）,hyperoside-2″-O-galloyl（Ⅶ）,hyperoside（Ⅷ）,kaempferol-3-O-D-glucopyranoside（Ⅸ）.Conclusion：Nine compounds are isolated for the first time from flowers of Koelreuteria paniculata.Compounds Ⅳ,Ⅴ,Ⅵ and Ⅸ are isolated from this genus for the first time.
出处
《中药材》
CAS
CSCD
北大核心
2011年第11期1716-1719,共4页
Journal of Chinese Medicinal Materials
关键词
栾树花
化学成分
Flowers of Koelreuteria paniculata Laxm.
Chemical constituents
