摘要
A C\-\{18\} RP packing with low adsorption was prepared by use of gelation reaction. Benzene, phthlene, phenanthrene, aniline and pyridine were selected as test solutes to evaluate the column with a mobile phase of 65% ACN aqueous solution. The performance and the stability were showed well after 1 000 column volume of 65% ACN aqueous solution(containing 0 1% TFA) .The strong polar alkine molecular can be separated well.
A C\-\{18\} RP packing with low adsorption was prepared by use of gelation reaction. Benzene, phthlene, phenanthrene, aniline and pyridine were selected as test solutes to evaluate the column with a mobile phase of 65% ACN aqueous solution. The performance and the stability were showed well after 1 000 column volume of 65% ACN aqueous solution(containing 0 1% TFA) .The strong polar alkine molecular can be separated well.
出处
《高等学校化学学报》
SCIE
EI
CAS
CSCD
北大核心
2000年第3期383-385,共3页
Chemical Journal of Chinese Universities
基金
国家自然科学基金!(批准号 :2 96 35 0 10 )
关键词
后凝胶化反应
高效液相色谱
反相填料
硅胶
Gellation reaction
High performance liquid chromatographic packing
Liquid chromatography
