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两步水浴法制备ZnO纳米棒阵列的研究 被引量：2

Study on ZnO Nanorod Arrays Prepared by a Two-Step Chemical Bath Deposition Method
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摘要 通过预加热处理完成了氧化锌(ZnO)种子层的制备,在种子层退火之后利用水浴法生长制备了排列有序的ZnO纳米棒阵列.采用扫描电子显微镜(SEM)、X射线衍射(XRD)和光致发光光谱(PL)分析了ZnO纳米棒阵列的表面形貌、结构和光学性质,考察了预处理温度和水洗时间对产物性能的影响.结果表明:预处理温度较低时无法形成ZnO种子层;制备的ZnO纳米棒阵列是纤锌矿结构;随着水浴时间的延长,ZnO纳米棒的长度逐渐增加. ZnO nanorod arrays are grown on silicon by chemical bath deposition.The seed layer is prepared by pre-heated,and then followed with chemical bath deposition.The morphology,structure and optical properties are characterized by SEM,XRD and PL.The results indicate that the prepared ZnO nanorod arrays are wurtzite structure,and the length of the ZnO nanorods increases with the length of the water bath time.
作者 刘春冉 张健 郑小东 陈雪娇
机构地区 华东师范大学信息科学技术学院
出处 《南通大学学报（自然科学版）》 CAS 2012年第1期30-34,共5页 Journal of Nantong University(Natural Science Edition)　
基金 国家自然科学基金项目(60672002 61076070) 上海市教育委员会科研创新项目(092246)
关键词 ZNO纳米棒 ZNO纳米棒阵列 水浴法 预加热 ZnO nanorod ZnO nanorod arrays chemical bath deposition pre-heated
分类号 TQ174.75 [化学工程—陶瓷工业]
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参考文献12

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二级参考文献23

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共引文献13

同被引文献17

  • 1刘娟,张跃,齐俊杰,贺建,黄运华,张晓梅.掺铟氧化锌纳米盘的制备、结构及性质研究[J].物理化学学报,2006,22(1):38-42. 被引量：15
  • 2孙成伟,刘志文,秦福文,张庆瑜,刘琨,吴世法.生长温度对磁控溅射ZnO薄膜的结晶特性和光学性能的影响[J].物理学报,2006,55(3):1390-1397. 被引量：42
  • 3阮伟东,王春旭,纪楠,徐蔚青,赵冰.化学气相沉积法制备ZnO纳米结构薄膜及其SERS活性研究[J].高等学校化学学报,2007,28(4):768-770. 被引量：20
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引证文献2

二级引证文献4

南通大学学报（自然科学版）
2012年 第1期

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