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高效液相色谱—串联质谱法同时测定水产品中19种磺胺类药物残留量 被引量:6

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摘要 针对水产品中磺胺类药物的多残留问题,建立了用高效液相色谱—串联质谱(HPLC-MS/MS)法同时测定水产品中19种磺胺类药物残留的方法。样品经匀浆后以乙酸乙酯为提取剂,提取液经正己烷脱脂,净化、浓缩后,用高效液相色谱—串联质谱法测定,氘代内标法定量。该方法可通过梯度洗脱,将具有相同定性离子的磺胺良好分离,方便快速,适用于批量样品的检测,检出限为1.0~10μg/kg,回收率为80%~105%,相对标准偏差(RSD)≤10%(n=5)。
出处 《水产科技情报》 北大核心 2012年第3期148-151,共4页 Fisheries Science & Technology Information
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