摘要
提出了X射线荧光光谱法测定闪速吹炼炉渣中8种痕量元素和4种组分的含量。将粒径为0.075～0.106mm的样品粉末以35t压力保压20s制成样片。选用标准样品绘制工作曲线,选择合适的测定谱线校正元素的谱线重叠干扰。用同一样品重复测定10次,测得其相对标准偏差小于6.5%。方法用于3个闪速吹炼炉渣样品分析,所得结果与其他方法的测定值相符。
XRPF determination of 8 trace elements and 4 components in slags from flash converting furnace was proposed in this paper. The sample was powdered to sizes in the range of 0. 075 0. 106 mm and pressed under a pressure of 35 t for 20 s to form a disc sample. Working curves were prepared by using standard samples. Interferences due to overlapping of spectral lines were overcomed by using suitable spectral lines. Values of RSD＇s （n= 10） were found to be less than 6.5% by analysis of a sample of flash converting furnace slag. Three samples were analyzed by the proposed method, giving results in consistency with the results found by other methods.
出处
《理化检验（化学分册）》
CAS
CSCD
北大核心
2012年第10期1216-1218,1232,共4页
Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
