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高速逆流色谱分离环氧化合物开环反应产物

Separation of Compounds from Epoxides Ring Opening Reaction Mixtures by High Speed Countercurrent Chromatography
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摘要 环氧苯乙烷在乙醇中与二正丁胺发生开环反应,反应体系经过初步处理,所得混合物应用高速逆流色谱分离纯化,得到目标产物β氨基仲醇,产物结构用1HNMR进行了确定。 β-amino alcohols were prepared by ring-opening of epoxides with dibutylamine use alcohol as solvent.The product was separated from the raction mixtures by HSCCC, and confirmed by 1HNMR.
作者 于文博 朱军
机构地区 杭州职业技术学院临江学院
出处 《科技视界》 2012年第29期165-165,252,共2页 Science & Technology Vision
关键词 高速逆流色谱 环氧化合物开环 分离纯化 HSCCC epoxide ring-openning Separation
分类号 O643.1 [理学—物理化学]
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科技视界
2012年 第29期

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