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风湿宁胶囊中挥发油的提取及包合工艺优选 被引量:10

Optimization of Extraction and Inclusion Technology for Volatile Oil from Anti-rheumatism Capsules
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摘要 目的:优选风湿宁胶囊中挥发油的提取与包合工艺。方法:采用水蒸气蒸馏法提取挥发油,以提取量为指标,通过单因素试验考察加水量、提取时间对提取工艺的影响;采用饱和水溶液法包合挥发油,以包合率为指标,通过正交试验考察挥发油与β-CD的比例、包合时间及包合温度对包合工艺的影响。结果:最佳提取工艺为加14倍量水提取4 h;最佳包合工艺为挥发油与β-环糊精的比例1∶8,包合温度40℃,包合时间3 h。结论:优选的挥发油提取与包合工艺条件稳定可行。 Objective:To optimize extraction and inclusion technology of volatile oil from anti-rheumatism capsules. Method: Volatile oil was extracted by steam distillation method,with yield of volatile oil as index,effect of water amount and extraction time on extraction technology was investigated by single factor test;Volatile oil was inclused by saturated aqueous solution method using inclusion ratio as index,orthogonal test was used to optimize inclusion technology with ratio of volatile oil to β-cyclodextrin,inclusion time and temperature as factors. Result: Optimum extraction conditions were:extracted 4 h with 14 times the amount of water;Optimal inclusion technology was as followings:ratio of volatile oil to β-cyclodextrin 1∶8,inclusion tempemture 40 ℃,inclusion time 3 h. Conclusion: These optimized extraction and inclusion technology conditions were reasonable and feasible.
出处 《中国实验方剂学杂志》 CAS 北大核心 2013年第5期22-24,共3页 Chinese Journal of Experimental Traditional Medical Formulae
基金 国家科技重大专项重大新药创制项目(2010ZX09102-210) 山西省科技产业化环境建设项目(2012061014-3)
关键词 风湿宁胶囊 挥发油提取 Β-环糊精 包合工艺 anti-rheumatism capsules extraction of volatile oil β-cyclodextrin inclusion technology
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