摘要
从药用植物小远志中提取、精制得多糖PP-1,PP-2,采用纸层析、薄层层析和气相色谱等方法确定了多糖中的单糖组成.通过高碘酸氧化、Smith降解和甲基化分析等方法确定了相邻单糖基连接方式,初步推测了两个小远志多糖可能的一级结构,为进一步合成和研究其生物活性提供了数据支持.
Two polysaccharides PP-1 and PP-2 were isolated and purified from Polygala sibirica L. var megalopha Fr. Their constituents were analyzed by paper chromatography, thin-layer chromatography (TLC) and gas chromatography (GC), and the link typies between monosaccharides were determined via periodate-oxidation, Smith degradation and methylation etc. Then their possible primary structure was inferred for the fixrther investigation of their synthesis and bioactivity.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2013年第2期365-369,共5页
Chinese Journal of Organic Chemistry
基金
江苏省高校自然科学(Nos.10KJA430050
11KJB150017)
江苏省普通高校研究生科研创新计划(No.CXZZ12_0979)资助项目~~
关键词
小远志多糖
组成
一级结构
Polygala sibirica L. var megalopha Fr. polysaccharide
composition
primary structure