摘要
本文介绍用化学共沉淀和在适当温度下煅烧以直接制备ＹＡＧ－Ａｌ２Ｏ３纳米复合粉体的新方法．ＸＲＤ结果表明，所得粉体具纯的ＹＡＧ和α－Ａｌ２Ｏ３相，因此其化学组成符合配料的组分设计．用本方法制备的２５ｖｏｌ％ＹＡＧ－Ａｌ２Ｏ３复合粉体经热压烧结，所得的致密体材料为晶内型纳米复合材料，其抗育强度达 ６１２ＭＰａ，断裂韧性为 ４．５４ＭＰａ·ｍ－１／２，都比单相 Ａｌ２Ｏ３陶瓷有大幅度提高。
vol%YAG-Al2O3 nanocomposite powders were prepared by the co-precipitaion method from ytrium nitrate and aluminium nitrate as starting materials. The XRD pattern for the prepared powder calcined at 1300 ℃ for 1h shows well-defined peaks whose positions are almost identical to those of stoichometic YAG and α-Al2O3. The powder compacts by hot-press sintering for 0.5 h at 1400 ℃ and 300MPa reached a density close to the thoretical, while the normally reported hot-press sintering temperature for YAG-Al2O3 composites is 1600 ℃. The bending strength and fracture toughness of prepared 25vol%YAG-Al2O3 nanocomposite were 612 MPa and 4.54 MPa·m-1/2, respectively, which are much higher than those of monolithic Al2O3 and monolithic YAG, as well as higher than those reported in other studies for YAG-Al2O3 composites. Microstructure studies found that the nano-YAG particles were mainly located within the Al2O3 grains.
出处
《无机材料学报》
SCIE
EI
CAS
CSCD
北大核心
2000年第6期1107-1110,共4页
Journal of Inorganic Materials
