摘要
目的建立参胶生血颗粒的质量控制方法。方法采用薄层色谱法对人参、黄芪、首乌进行定性鉴别;用HPLC-ELSD法测定黄芪甲苷的含量。结果薄层色谱斑点清晰集中,易于鉴别;黄芪甲苷进样量在0.021～0.063μg范围内线性关系良好(r=0.9998),平均加样回收率为98.95%(RSD=1.27)。结论本方法灵敏、准确、重现性好、专属性强,可作为参胶生血颗粒的质量控制提供依据。
Objective To establish the method for quality control of Shenjiao Shengxue granule. Methods Ren Shen, Huang Qi and He Shou Wn were identified by TLC. The content of astragaloside iv was determined by HPLC- ELSD. Results The spots of TLC were clear and concentrative. There was a good linear relationship for astragaloside iv with the ranges of 0.021-0.063μ g（r=0.9998）. Their average recoveries were 98.95% （RSD=1.27）. Conclusion This method is sensitive, accerate, reproducible and exclusive.
出处
《中国医药科学》
2013年第6期98-100,共3页
China Medicine And Pharmacy
