摘要
目的:优选党参的亚临界水提取工艺。方法:以党参炔苷和党参多糖提取率的综合评分为指标,采用单因素试验和正交试验考察料液比、提取时间和温度对党参亚临界水提取工艺的影响,并与传统提取工艺进行比较。结果:最佳亚临界水提取工艺为提取温度150℃,提取时间45 min,料液比12 mL.g-1;党参炔苷和党参多糖的提取率分别达0.110 2,195.1mg.g-1。结论:与传统水煎煮工艺相比,优选的工艺可明显降低提取时间,并显著提高党参炔苷和党参多糖的提取率。
Objective: To optimize subcritical water extraction technology of Codonopsis tangshen. Method: With composite score of yield of lobetyolin and polysaccharides from C. tangshen as index,effects of liquid-solid ratio,extraction time and temperature on subcritical water extraction technology was investigated by single-factor tests and orthogonal test,and compared with traditional extraction technology. Result: Optimum extraction conditions were obtained as follows:extraction temperature 150 ℃,liquid-solid ratio 12 mLg-1,extraction time 45 min;Under these conditions,yield of lobetyolin and polysaccharides from C. tangshen was up to 0.110 2,195.1 mgg-1, respectively. Conclusion: Comparing with conventional water boiling technology,this optimized technology could significantly shorten extraction time and significantly improve yield of lobetyolin and polysaccharides from C. tangshen.
出处
《中国实验方剂学杂志》
CAS
北大核心
2013年第10期34-37,共4页
Chinese Journal of Experimental Traditional Medical Formulae
基金
江西省教育厅青年科学基金项目(GJJ11186)
关键词
党参
亚临界水提取
党参炔苷
党参多糖
正交试验
Codonopsis tangshen
subcritical water extraction
lobetyolin
polysaccharides from Codonopsis tangshen
orthogonal test