摘要
目的完善坤复康胶囊的质量标准。方法采用TLC法鉴别制剂中的苦参和乌药,HPLC法测定制剂中的α-香附酮含量。结果方法的专属性、重复性和稳定性良好,α-香附酮对照品在8.876 ng^221.9 ng范围内呈线性关系,γ=0.9999,平均回收率为98.9%,RSD为0.71%(n=7)。结论完善后的质量标准可行,能有效控制坤复康胶囊的质量。
Objective to perfect the quality standard of Kun Fu Kang capsule. Method for identification of Radix So- phorae Flavescentis and preparation of the TLC method was used in the preparation, determination of alpha - cyperone content with HPLC method. Results the specificity, repeatability and stability of the method were good, alpha - cyperone control in 8. 876 ng~ 221.9 ng was linear in the range, γ =0.9999, the average recovery was 98.9 %, RSD was 0.71% （ n = 7）. Conclusion the improved quality standard of the feasible, can effectively control the quality of Kun Fu Kang cap- sule.
出处
《现代中医药》
CAS
2013年第6期81-83,共3页
Modern Chinese Medicine
基金
国家药典委员会药品标准提高计划项目(2012)
关键词
坤复康胶囊
质量标准
Α-香附酮
Kun Fu Kang capsule
quality standard
alpha -cyperone
