摘要
建立了电感耦合等离子体发射光谱法测定食品中硼含量的方法。通过比较湿法消解、干法消解和微波消解三种前处理方法对测定硼含量的结果，结果发现样品的微波消解前处理方法效果最佳。在仪器最佳操作条件下，食品中硼含量检测的线性范围在0-2mg／L之间；检出限（LOD5）为0．00254mg／L；回收率在89．00％-97．50％之间；相对标准偏差（RsD）〈5．0％。该方法具有准确灵敏、简捷快速的特点，能够应对大量食品中硼含量的抽检任务。
Inductively coupled plasma atomic emission spectromeuy determination of boron content in food. By comparing the wet digestion, dry digestion and microwave digestion the results of the three pre-trealment method for the determination of boron content and found that the microwave digestion of the sample pre-treatment method works best. In optimum operating conditions, the linear range of detection of the boron content in food in between 0 to 2 mg / L, limit of detection （LODs） is 0.002 54 mg/L, recoveries in the range of 89.00% to 97.50%, relative standard deviation （RSD） 〈5.0%,4. The method is accurate and sensitive, simple and quick, able to cope with a large number of food sampling of boron task.
出处
《食品工业》
北大核心
2013年第12期223-226,共4页
The Food Industry
基金
嘉兴市科技计划项目(2011AY1042
2012AY1017)
浙江省质量技术监督系统科研计划项目(20110231)
关键词
电感耦合等离子体发射光谱法
硼
前处理方法
微波消解
inductively coupled plasma emission spectrometry
boron
pretreatment methods
microwave digestion
