摘要
目的：建立艾纳香挥发油栓的质量控制标准.方法：采用薄层色谱法对艾纳香进行定性鉴别,气相色谱法测定龙脑含量.结果：薄层鉴别可以检测出艾纳香对应的斑点,斑点清晰,阴性对照无干扰;龙脑对照品在0.025～1.60mg·mL-1之间线性关系良好（r2=0.9997）,平均回收率为98.34％（RSD为0.42％,n=6）.结论：该方法操作简单,准确性高,重复性好,可用于该制剂的质量控制.
Objective. To establish the quality standard for the Blumea volatile oil suppository. Methods ： Used the ways of TLC to differentiate Blumea in suppository. GC ways to measure the content of BorneoL Results： The analysis of TLC showed that the sam- pie and contrast have same color spots with similar RF value. Borneol was linear in the concentration range of 0. 025-1.60mg？ roL- l （r2 = 0.9997）, and the average recover was 98.34 % （RSD= 0.42%, n = 6 ） Conclusion .. The methods were simple, accurate, re- producible, and can be used for the quality control of this preparation.
出处
《亚太传统医药》
2014年第5期35-38,共4页
Asia-Pacific Traditional Medicine
关键词
艾纳香
挥发油栓
质量标准
Blumea
Volatile Oil Suppository
Quality Control
