摘要
本文介绍了以亚硝酸乙酯代替亚硝酸丁酯 ,用氯苯代替无水乙醚合成铜铁试剂的新工艺。该法消除了原工艺中存在的一些弊病 ,对影响反应的诸因素进行了详细讨论 ,为该产品的工业化生产提供可靠数据 ,产品总收率 5 0 %左右。
In stead of using butyl nitrite and absolute ethyl-ether as reagents,in an improved method,cupferron.(aminoium N-nitroso-phenylhydroxy amine)was synthesized by using ethyl nitrite and chlorobenzene.The new synthetic method could remove some shortness happened in the old technology.Some experimental parameters were discussed.The yield of cupferron was about 50%.
出处
《化学与粘合》
CAS
2001年第1期39-40,共2页
Chemistry and Adhesion
