摘要
目的：建立鹰不泊药材的品质评价方法和橙皮苷含量测定方法。方法：按照《中国药典》2010年版一部附录方法测定其水分、灰分及浸出物含量；采用HPLC法测定橙皮苷的含量。结果：7个不同产地鹰不泊药材水分含量范围为7.27%~9.65%；总灰分含量范围为5.28%~7.90%；酸不溶性灰分范围为0.39%~0.86%；水溶性浸出物含量范围为冷浸法5.95%~10.72%，热浸法7.05%~12.13%；乙醇浸出物含量范围为冷浸法5.88%~10.92%，热浸法8.16%~12.67%；40%乙醇浸出物含量范围为冷浸法3.85%~4.97%，热浸法2.38%~3.83%；橙皮苷含量范围为0.40%~2.68%。结论：所建立方法可用于鹰不泊药材的品质评价。
Objective：To establish the methods for the quality evaluation and hesperidin content determination of Radix Zanm-thoxyli Avicennae. Methods： The moisture, ash and extract content was respectively detected according to the methods described in Chinese Pharmacopoeia 2010 edition, and the content of hesperidin was detected by HPLC. Results： The moisture contents of Radix Zanmthoxyli Avicennae from seven different areas were between 7. 27% and 9. 65%; the total ash contents were between 5. 28% and 7. 90%;the acid-insoluble ash content were between 0. 39% and 0. 86%;the water-soluble extract contents were within the range of 5. 95%-10. 72% by infusion and 8. 16%-12. 67% by hot dipping;the alcohol extract contents were within 5. 88%-10. 97% by infu-sion and 2. 38%-3. 83% by hot dipping. The content of hesperidin was 0. 40%-2. 68%. Conclusion：The established methods can be used to evaluate the quality of Radix Zanmthoxyli Avicennae.
出处
《中国药师》
CAS
2014年第4期544-545,584,共3页
China Pharmacist
基金
广东省中医药强省项目(编号:20122073)
关键词
鹰不泊
质量标准
橙皮苷
HPLC法
Radix Zanmthoxyli Avicennae
Quality evaluation
Hesperidin
HPLC
