摘要
目的建立久强脑立清中薄荷脑、龙脑的含量测定方法。方法采用GC法，用PEG-20M10％涂布浓度色谱柱，载气：氮气，检测器：氢火焰离子化检测器（FID）。结果薄荷脑在0．02024～1．012mg·ml^-1范围内，回归方程为Y=32．10X＋45．30，r=0．9997。龙脑在0．02006～1．003mg·ml^-1范围内，回归方程为Y=21．32X＋51．11，r=0．9992，两化合物在相应浓度范围内具有良好的线性关系。结论该方法简便快捷，准确、重复性好，灵敏度高，可用于建立久强脑立清的质量控制。
Objective To establish an assay quality standard for Jiuqiang Naoliqing. Methods GC was used to determine the content of menthol and borneol. Results A good linearity was seen in the range of 0. 020 24 - 1. 012 μg（ r =0. 9997） of menthol and in the range of 0. 020 06 - 1. 003μg（ r =0. 9992） of borneol. The recov-ery was up to the standard. Conclusion This method is simple and stable,which can be used for quality control of Jiuqiang Naoliqing.
出处
《解放军药学学报》
CAS
2014年第2期148-150,共3页
Pharmaceutical Journal of Chinese People's Liberation Army
