摘要
研究Te共沉淀分离富集、ICP-MS铂族元素和金测定方法。方法检出限 1~9 pg/g;回收率≥90%。国标GBW07288-GBW07294、加拿大WGB1及南非铂矿SARM7等标样分析表明:结果满意,方法可靠。
A method for the determination of Pt.Pd. Ru. Rh. Ir and Au in geological samples was studied. The sample was fused by sodium peroxide and determined by a double focusing high resolution inductively coupled plasma mass spectrometer 'ELEMENT' after the separation and enrichment by co-precipitation with Te. Detection limit of the method was between 1 -9ng/g and the recovery was > 90%. Our analytical results for some domestic or international reference materials were in agreement with the certified values.
出处
《分析化学》
SCIE
EI
CAS
CSCD
北大核心
2001年第6期653-656,共4页
Chinese Journal of Analytical Chemistry