摘要
We have synthesized [Bi(C 5H 10 NO 2S) 2ClH 2O] complex using the solide phase reaction of DL methiomine with bismuth trichloride.Its composition and structure have been characterized by the chemical analysis,elemental analysis,IR spectra and X ray powder diffraction.The XRD patterns have been indexed.The results show that the complex is of monoclinic system and the lattice parameters are:a=1.6166nm,b=0.7214nm,c=1.5448nm,β=94.68°,V=1.7956nm 3,Z=4,D exp =2.067g·cm -3 ,D cal =2.049g·cm -3 .
We have synthesized [Bi(C 5H 10 NO 2S) 2ClH 2O] complex using the solide phase reaction of DL methiomine with bismuth trichloride.Its composition and structure have been characterized by the chemical analysis,elemental analysis,IR spectra and X ray powder diffraction.The XRD patterns have been indexed.The results show that the complex is of monoclinic system and the lattice parameters are:a=1.6166nm,b=0.7214nm,c=1.5448nm,β=94.68°,V=1.7956nm 3,Z=4,D exp =2.067g·cm -3 ,D cal =2.049g·cm -3 .
出处
《化学研究与应用》
CAS
CSCD
北大核心
2002年第2期205-207,共3页
Chemical Research and Application
