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固相萃取光度法测定烟草中的挥发酚 被引量:11

Determination of volatile phenol in tobacco with solid phase extraction spectrophotometry
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摘要 研究了用WatersSep Park C1 8固相萃取小柱萃取测定烟草样品中的挥发酚的方法。用自动水蒸汽蒸馏仪蒸馏出烟草样品中的挥发酚 ,4 氨基安替比林显色 ,显色产物可用WatersSep Park C1 8固相萃取小柱萃取 ,以乙醇洗脱后用分光光度法测定 。 A method for determination of volatile phenol in tobacco by solid phase extraction spectrophotometry was studied. Volatile phenol in tobacco was separated by distillation, and reacted with 4-aminoantipyrinethe. The colored product was determined by spectrotometry after extracted by Waters Sep-Park-C_ 18 column and eluted by ethanol. The method was applied to determination of volatile phenol in tobacco samples with satisfactory results.
出处 《分析试验室》 CAS CSCD 北大核心 2002年第2期31-32,共2页 Chinese Journal of Analysis Laboratory
关键词 测定 烟草 挥发酚 固相萃取 光度法 质量 Totacco volatile phenol Solid phase extraction spectrophotometry
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