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纳米Hg_2Cl_2/Al_2O_3有序阵列体系的制备和表征 被引量:2

Synthesis and Characterization of Nano-Hg_2Cl_2/Al_2O_3 Ordered Array System
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摘要 We have prepared ordered porous alumina membrane. Metal Zn was deposited within the pores of alumina membrane by direct current. The alumina membrane with Zn in the pores was immersed in HgCl 2 solution and Hg 2Cl 2/Al 2O 3 ordered array was synthesized by utilizing Zn reduced HgCl 2. The XRD and TEM measuring demonstrated Hg 2Cl 2 located in the pores of alumina membrane and the diameters range from 30 to 80 nm. We have prepared ordered porous alumina membrane. Metal Zn was deposited within the pores of alumina membrane by direct current. The alumina membrane with Zn in the pores was immersed in HgCl 2 solution and Hg 2Cl 2/Al 2O 3 ordered array was synthesized by utilizing Zn reduced HgCl 2. The XRD and TEM measuring demonstrated Hg 2Cl 2 located in the pores of alumina membrane and the diameters range from 30 to 80 nm.
出处 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 2002年第7期1401-1403,共3页 Chemical Journal of Chinese Universities
基金 国家自然科学基金 (批准号 :199740 41) 安徽省教育厅自然科学基金资助
关键词 Hg2Cl2/Al2O3 模板合成 有序阵列 电沉积 甘汞电极 纳米材料 氯化汞 氧化铝 Template synthesis Calomel Ordered array Electrodeposition
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