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3种福建省柚子汁挥发性成分及香气分析 被引量:13

Analysis of the Volatiles and Aroma of the Juice of Three Varieties of Pummelo in Fujian Province
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摘要 利用固相微萃取结合气相色谱质谱联用(GC-MS)技术检测了溪蜜柚汁、平和红柚汁、度尾文旦柚汁的挥发性成分,并计算了这3种柚汁中各挥发性成分的香气值.结果显示,溪蜜柚汁、平和红柚汁、度尾文旦柚汁中分别检测出了23种、17种、16种挥发性成分,其中溪蜜柚汁中含量最高的成分为反式-3-己烯-1-醇(765.26μg/L),平和红柚汁中含量最高的成分为正己醛(175.21μg/L),度尾文旦柚汁中含量最高的成分为d-柠檬烯(21.99μg/L).柚汁香气值计算结果显示,溪蜜柚汁香气值较大的成分为1-辛烯-3-醇、正己醛、2-甲基丁酸乙酯等,香气主要表现为蘑菇气味、青草气味、香甜气味等;平和红柚汁香气值较大的成分为正己醛、癸醛、顺式-3-己烯醛、辛醛、芳樟醇等,香气主要具有青草气味、水果气味、柑橘气味、香甜气味等;度尾文旦柚汁香气值较大的成分为癸醛和正己醛,香气主要由水果气味和青草气味组成. Volatiles of Guanxi pummelo juice, Pinghe were extracted by solid-phase micro-extraction and analyzed by trometer (SPME -GC -MS), and their odor activity values 16 volatile compounds were identified and quantified in these (765.26 μg/L) was the most dominant volatile component in red pummelo juice and Duwei pummelo juice gas chromatography equipped with a mass spec- (OAVs) were calculated. A total of 23, 17, three juices, respectively. (E) -3-hexen-l-ol Guanxi pummelo juice. However, Pinghe redpummelo juice was rich in hexanal (175.21 μg/L). High concentration of d-limonene (21.99 μg/L) was found in Duwei pummelo juice. According to the results of odor activity values, 1-octen-3-ol, hexanal and ethyl 2-methylbutanoate were the odour characteristic components, creating mushroom, green, floral and sweet odor in Guanxi pummelo juice. Hexanal, decanal, (Z)-3-hexenal, octanal and linalool were the characteristic aroma components of Pinghe red pummelo juice, contributing to the green, fruit, lemon, floral and sweet notes of its aroma. In Duwei pummelo juice, decanal and hexanal were detected as potent odorants with fruit and green aroma.
出处 《集美大学学报(自然科学版)》 CAS 2014年第4期266-273,共8页 Journal of Jimei University:Natural Science
基金 国家自然科学基金资助项目(31371751) 厦门市杰出青年科学基金项目(3502Z20126008) 集美大学科研创新团队基金项目(2010A006) 福建省教育厅基金资助项目(JA12188)
关键词 固相微萃取 气相色谱质谱联用 挥发性成分 柚子汁 SPME GC - MS volatiles pummelo juice
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参考文献20

  • 1张怡,曾绍校,冯翀,郑宝东.福建省主栽柚子品种营养与保健成分的分析[J].营养学报,2008,30(5):520-522. 被引量:8
  • 2NARDINI G S, MERIB J O, DIAS A N, et al. Determination of volatile profile of citrus fruit by HS-SPME/GC-MS with oxidized NiTi fibers using two temperatures in the same extraction procedure [ J]. Microchemical Journal, 2013, 109: 128-133.
  • 3CHEONG M W, ZHU D, SNG J, et al. Charucterisation of calamansi (Citrus microcarpa) Part II: volatiles, physico- chemical properties and non-volatiles in the juice [ J]. Food Chemistry, 2012, 134(2) : 696-703.
  • 4JABALPURWALA F, GURBUZ O, ROUSEFF R. Analysis of grapefruit sulphur volatiles using SPME and pulsed flamephotometric detection [ J]. Food Chemistry, 2010, 120(1) : 296-303.
  • 5BIANCHI F, CARERI M, MANGIA A, et al. Characterization of the volatile profile of orange juice contaminated with AI- icyclobacillus acidoterrestris [ J]. Food Chemistry, 2010, 123 (3) : 653-658.
  • 6吴继红,张美莉,陈芳,廖小军,胡小松.固相微萃取GC-MS法测定苹果不同品种中主要芳香成分的研究[J].分析测试学报,2005,24(4):101-104. 被引量:72
  • 7王丽霞,钟海雁,袁列江.固相微萃取法提取果汁香气的影响因素及萃取条件的优化[J].安徽农业科学,2006,34(15):3787-3788. 被引量:27
  • 8BARBONI T, LURO F, CHIARAMONTI N, et al. Volatile composition of hybrids Citrus juices by headspace solid-phase micro extraction/gas chromatography/mass spectrometry[J] Food Chemistry, 2009, 116(1): 382-390.
  • 9YEOM H W, STREAKER C B, ZHANG Q H, et al. Effects of pulsed electric fields on the quality of orange juice and comparison with heat pasteurization [ J ]. Journal of Agricultural and Food Chemistry, 2000,48 (10) : 4597-4605.
  • 10VAN DEN DOOL H, DEC KRATZ P. A generalization of the retention index system including linear temperature pro- grammed gas-liquid partition chromatography [ J]. Journal of Chromatography A, 1963, 11 : 463-471.

二级参考文献21

  • 1吴继红,张美莉,陈芳,廖小军,胡小松.固相微萃取GC-MS法测定苹果不同品种中主要芳香成分的研究[J].分析测试学报,2005,24(4):101-104. 被引量:72
  • 2YANG X,PEPPARD T L.Solid-Phase Microextraction of flavor compounds-a comparison of two fiber coatings and a discussion of the rule of thumb for adsorpotion[J].LC-GC,1995,13:882-886.
  • 3YANG X,PEPPARD T L.For flavor analysis[J].Agr Food Chem,1994,42:1925-1930.
  • 4PAN L,ADAMS M.Pawliszyn.Determination of fatty acids using solid-phase microextraction[J].Anal Chem,1995,67:4 396-4 403.
  • 5PAN L,PAWLISZYN.Deriveration/solid-phase microextraction:new approach to polar analytes[J].Anal Chem,1997,69:196-205.
  • 6BUCHHOLS K D.Optimalzation of solid-phase microextraction condition for determination of phenola[J].Anal Chem,1994,65:160-167.
  • 7PAN L,PAWLISZYN.Determination of fatty acids using solid-phass microextraction[J].Anal Chem,1995,67:4 396.
  • 8LOUCH D.Dynamics of organic compound extraction from water using liquid chromatograph[J].Anal Cham,1992,64:1 187-1 199.
  • 9杨月欣.中国食物成分表2004[M].北京:北京大学医学出版社,2006.213.
  • 10张道宁,吴采樱,艾飞.固相微萃取中高分子涂层的研究[J].色谱,1999,17(1):10-13. 被引量:47

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