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超声提取-电感耦合等离子体质谱法快速测定卷烟纸中钾、钠、钙、镁的含量 被引量:13

Rapid Determination of Potassium, Sodium, Calcium, and Magnesium in Cigarette Paper with Ultrasonic Extraction-Inductively Coupled Plasma Mass Spectroscopy Method
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摘要 采用超声提取-电感耦合等离子体质谱法能快速测定卷烟纸中钾(K)、钠(Na)、钙(Ca)、镁(Mg)含量,控制卷烟纸的质量稳定性。检出限分别为2.46、0.44、8.84、0.28μg/L;回收率90.3%-109.0%;相对标准偏差(RSD)〈5%。此方法具有操作简单、准确、快速等优点,适合于卷烟纸中K、Na、Ca、Mg含量的分析。 In order to monitor cigarette paper quality, the contents of potassium (K), sodium (Na), calcium (Ca) and magnesium (Mg) in cigarette paper were rapidly detected by ultrasonic extraction-inductively coupled plasma mass spectroscopy method. The LODs of K, Na, Ca and Mg were 2.46, 0.44, 8.84 and 0.28 μg/L, respectively. The recoveries were in range of 90.3%-109.0%, with RSD less than 5%. This method is simple, fast and accurate, and suitable for detecting K, Na, Ca and Mg in cigarette paper.
出处 《中国烟草科学》 CSCD 2014年第3期79-84,共6页 Chinese Tobacco Science
关键词 超声提取 电感耦合等离子体质谱法 卷烟纸 ultrasonic extraction inductively coupled plasma mass spectroscopy cigarette paper potassium sodium calcium magnesium
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