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微硅粉制取高纯白炭黑的工艺初探 被引量:8

Preparation of High-purity Silica White Using Micro-silica Powder
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摘要 研究了以微硅粉碱性焙烧-熟料浸出-溶液净化-碳分沉淀-洗涤-干燥-煅烧工艺制取白炭黑。将微硅粉与纯碱混合均匀,在850℃下焙烧1 h制成偏硅酸钠熟料;熟料水浸得偏硅酸钠溶液;偏硅酸钠溶液在水浴温度70℃下,用石灰粉搅拌净化1 h除杂,净化液中杂质Fe脱除率为94%,Al脱除率为56%,SiO2损失率为19%;净化液用CO2碳分沉淀,控制温度50~60℃,CO2流量与空气流量比为1∶7~1∶7.5,碳分时间3~4h,获得颗粒均匀的偏硅酸沉淀;偏硅酸经盐酸及蒸馏水洗涤后干燥煅烧得高纯白炭黑,白炭黑纯度在99.98%以上。此工艺原料易得,过程控制简单,不产生污染,可实现工业微硅粉的高值化利用。 Preparation of high-purity silica white by micro-silica powder roasting with alkaline clinker -leaching using water -solution purification -carbon dioxide decomposition -washing -calcination has been researched .The mixture of micro-silica powder with soda was roasted at 850 ℃ for 1 hour to prepare sodium metasilicate clinker .The clinker was leached with water at temperature of 70 ℃ ,then the impurity(Al ,Fe) in the leaching solution was removed with lime powder .Removal rate of Fe is 94% ,removal rate of Al is 56% ,the loss rate of SiO2 is 19% .The purified solution was carbon decomposition for 3-4 hours using CO2 to precipitate acid metasilicate at temperature of 50-60 ℃ , CO2 flow and air flow ratio of 1∶7 .0 -1∶7 .5 .The precipitated acid metasilicate was washed using hydrochloric acid and distilled water ,then was dried and calcined to obtain high-purity silica white with SiO2 grade over 99 .98% .For process ,the raw materials are readily available ,process is simple , no-pollution ,industrial silica powder can be fully used with high value .
机构地区 昆明冶金研究院
出处 《湿法冶金》 CAS 北大核心 2014年第5期406-409,共4页 Hydrometallurgy of China
关键词 微硅粉 焙烧 浸出 洗涤 煅烧碳分 高纯白炭黑 micro-silica powder roasting leaching washing calcining carbon decomposition silica w hite
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