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原子吸收光谱法测定连铸保护渣中的铁

The Determination of Iron Content in Metallurgy Continuous Casting Powder by Atomic Absorption Spectrometry
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摘要 介绍了通过原子吸收光谱法测定保护渣中铁含量的方法并对试液的酸度、共存离子的干扰、试样分解条件以及测量范围等测量条件进行了分析和讨论。结果表明,该方法的加标回收率为98.0%-102.7%,相对标准偏差小于2%(n=11),测定的灵敏度、准确度、精密度均能满足保护渣日常检验分析的要求。 A method was introduced that the content of the iron in metallurgy continuous casting was determined by atomic absorption spectrometry and its influencing factors and results were discussed. The results showed that the recovery rate was 98. 0% - 102. 7%,and the relative standard deviation( RSD) was less than 2%. Absorption spectrometry was a fast and simple method with high accuracy and sensitivity,which could be used for the quality control of iron in metallurgy continuous casting powder.
出处 《广州化工》 CAS 2014年第21期128-130,共3页 GuangZhou Chemical Industry
关键词 保护渣 原子吸收光谱法 metallurgy continuous casting powder atomic absorption spectrometry iron
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参考文献4

  • 1鞍钢钢研所,沈阳钢研所.实用冶金分析-方法与基础[M].沈阳:辽宁科技出版社,1990.
  • 2重金属冶金分析手册编写组.重金属冶金分析[M].北京:冶金工业出版社,1994.
  • 3范建.原子吸收分光光度法[M].长沙:湖南科技出版社,1981.
  • 4邓勃.原子吸收光谱分析的原理[M].北京:清华大学出版社.

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