摘要
为了研究萘乙酸在黄瓜中的残留量，建立了黄瓜中萘乙酸的高效液相色谱方法。样品在酸性条件下用乙腈提取后过C18固相萃取小柱，用甲醇：水：磷酸为60：40：0．35的流动相洗脱，用C18液相色谱柱和带有紫外检测器的液相色谱检测。结果表明，添加水平在0．02，0．1mg／kg下回收率为90％-110％，该方法操作简单、快速，灵敏度高。
To study residue of cucumber, a method of cucumber naphthvlacetic by High Performance Liquid Chromatography is developed. Samples under acid condition after were extracted with acetonitrile C18 solid phase extraction column, and then tested by methanol ： water ： phosphoric acid was 60 ： 40 ： 0.35 mobile phase elution with C18 column of liquid chromatography and liquid chromatography with UV detector, adding level under the concentration of 0.02, 0.1 mg/kg recovery from 90% to 110%. This method is easy, fast, and high sen sitivity.
出处
《山西农业科学》
2014年第11期1172-1174,共3页
Journal of Shanxi Agricultural Sciences
