摘要
建立了采用气相色谱-质谱联用技术快速、准确测定近林地水中敌敌畏残留量的方法。采用液液提取的方式对水样进行前处理,提取后使用气质联用仪进行分析。该方法选择性好,灵敏度高,敌敌畏检测线性范围为0.05~1.0mg·L^(-1),检出限为0.02mg·L^(-1),加标回收率在92.5%~97.9%之间,可以作为近林地水样中敌敌畏残留量的检测和确证方法。
A rapid and accurate method for determination of dichlorvos residues in water near fruit bearing forest was established by gas chromatography-mass spectrometry. The samples were determined by GC-MS after liquid-liquid extraction. The linear range of the method was 0.05~1.0mg/L, the determination limit was 0.02mg/L, and the recovery was 92.5%~97.9%. The proposed method had good selectivity and high sensitivity, and was suitable for analysis of dichlorvos residues in water near fruit bearing forest.
作者
韩璐
黄大波
HAN Lu HUANG Dabo(Department of Chemical Engineering, Yingkou Institute of Technology, Yingkou 115014, China Criminal Police Detachment of Yingkou Public Security Bureau, Yingkou 115000, China)
出处
《化工技术与开发》
CAS
2017年第6期46-47,51,共3页
Technology & Development of Chemical Industry
关键词
气相色谱
质谱
敌敌畏
测定
gas chromatography
mass spectrometry
dichlorvos
determination
