期刊文献+

荧光检测-高效液相色谱法测定水质中生物胺 被引量:6

Water Quality-Determination of Biogenic Amine by HPLC-FLD
下载PDF
导出
摘要 本文以常存在于水中的五种生物胺(腐胺PUT.、尸胺CAD.、组胺HIS.、亚精胺SPD.、精胺SPM.)作为分析对象,优化了液相色谱的测定条件(流动相、发射波长、梯度洗脱程序等)、生物胺的衍生条件以及分散液液微萃取的萃取条件,建立了分散液液微萃取-液相色谱-荧光检测技术应用于检测水中五种生物胺残留的方法。 This paper analyzes five biogenic amine ( putrescine , cadaverine , histamine, spermidine , spermine ) which are often found in water. Conditions about liquid chromatography (mobile phase, emission wavelength, gradient elution procedures) and conditions about derivatization and conditions about dispersive liquid-liquid mieroextraetion are all optimized. Finally, we have built a technology about DLLME-HPLC-FLD which can be used to test the concentration of biogenic amine in water.
出处 《福建分析测试》 CAS 2018年第1期35-38,共4页 Fujian Analysis & Testing
基金 福建省科技计划项目公益类科研院所基本科研专项资助(2015R1007-1)
关键词 生物胺 高效液相色谱-荧光检测 液液微萃取 biogenic amine HPLC-FLD DLLME
  • 相关文献

参考文献2

二级参考文献38

  • 1龚慕辛,宋亚芳,王智民,张启伟,闫利华,朱晶晶.吴茱萸化学成分的研究[J].中国中药杂志,2009,34(6):792-794. 被引量:28
  • 2李志军,薛长湖,吴永宁.反相高效液相色谱法测定食品中生物胺[J].食品工业科技,2005,26(4):175-178. 被引量:25
  • 3黄梅丽 汇小梅.食品化学[M].中国人民大学出版社,1989..
  • 4Cinquina A,Caly A,Longo F,et al.Determination of biogenic amines in fish tissues by ion-exchange chromatography with conductivity detection[J].Journal of Chromatography A,2004,1032:73-77.
  • 5Shalaby A R.Significance of biogenic amines to food safety and human health[J].Food Research International,1996,29:675-690.
  • 6Eerola S,Hinkkanen R,Lindfors E,et al.Liquid chromatographic determination of biogenic amines in dry sausage[J].Journal of AOAC International,1993,76:575-577.
  • 7Hernandez-Jover T,Izquierdo-Pulido M,Veciana-Nogues M T,et al.Effect of starter cultures on biogenic amine formation during fermented sausages production[J].Journal of Food Protection,1997,60:825-830.
  • 8Ordonez A I,Iban.F C,Torre P,et al.Formation of biogenic amines in Idiazabal ewe's milk cheese:effect of ripening,pasteurization,and starter[J].Journal of Food Protection,1997,60:1371-1375.
  • 9Vinci G,Anonelli M L.Biogenic amine:qualiIy index of freshness in red and white meat[J].Food Control,2002,13(3):519-524.
  • 10Martin K,Frantisek V,Lenka V,et al.Biogenic amines in vacuum-packed and non-vacuum-packed flesh of carp (Cyprinus carpio) stored at different temperatures[J].Food Chemistry,2004,88:185-191.

共引文献43

同被引文献75

引证文献6

二级引证文献16

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部