摘要
研究超声波提取法提取桔梗中残留的克百威农药,探讨了提取时间、提取温度和所加溶剂量对克百威提取率的影响,并通过正交设计对桔梗中药的克百威提取条件进行优化.结果表明提取温度、提取时间和溶剂量对克百威的提取均有显著影响.通过方差分析,确定其影响因素的大小顺序是提取温度>提取时间>溶剂量.最优提取条件为温度40℃、丙酮溶剂量30 m L、提取时间30 min.
The ultrasonic extraction method for extraction of carbofuran pesticide from platycodon grandiflorum was studied. The effects of extraction time, extraction temperature and the amount of solvent on the extraction rate of carbofuran were discussed. The extraction condi-tions of platycodon grandiflorum were optimized by orthogonal design. The extraction temper-ature ,extraction time and solvent content have a significant effect on the extraction of carbo- furan. Through the analysis of variance, the order of the influencing factors was determined as follows ： extraction temperature 〉 extraction time 〉 solvent quantity. The optimum extrac-tion conditions were ： temperature of 40 ℃ , acetone solvent amount of 30 mL and extraction time of 30 min.
作者
郎朗
王戈
石磊
狄静波
LANG Lang , WANG Ge, SHI Lei, DI Jing-bo(1. Post - doctoral Research Mobile Station of Chinese Materia Medica, Harbin University of Commerce, Harbin 150076, China; 2. Research Center of Life Sciences and Environmental Sciences, Harbin University of Commerce, Harbin 150076, China;)
出处
《哈尔滨商业大学学报（自然科学版）》
CAS
2018年第2期143-146,共4页
Journal of Harbin University of Commerce：Natural Sciences Edition
基金
哈尔滨市青年项目(2013RFQXJ054)
2016年哈尔滨商业大学青年创新人才支持项目(2016QN058)
黑龙江省教育厅科学技术研究项目(12541188)
关键词
克百威
桔梗
超声提取法
农药残留
carbofuran
campanulaceae
ultrasonic extraction
pesticide residues
