摘要
选取麻醉抢劫案中常见的七种苯二氮杂卓类药物——安定、利眠宁、硝基安定、氯硝安定、艾司唑仑、阿普唑仑和三唑仑为研究对象,通过定性、定量分析,从色谱行为、不同检测器相关系数及线性关系、方法精密度、检出限等四方面,对比了气相色谱氮磷检测法和气相色谱质谱法的检测效果。结果表明,氮磷检测法在方法的灵敏度、精密度、线性相关性都明显好于质谱检测法。
Seven kinds of benzodiazepine drugs,sedoxan,chlorhexidine,nitrazepam,clonazepam,estazolam,alprazolam and triazolam,were selected as the research object. Qualitative and quantitative analysis were used to compare the detection of gas-chromatography nitrogen-phosphorus detection and gas chromatography-mass spectrometry from the aspect of chromatographic behavior,correlation coefficient and linear relationship. The results showed that gas-chromatography nitrogen-phosphorus detection were significantly better than mass spectrometry in sensitivity,precision,linear correlation.
作者
栾陈杰
陈筱月
吴国萍
LUAN Chen-jie;CHEN Xiao-yue;WU Guo-ping(Criminal Science and Technology Department Jiangsu Police Institution,Jiangsu Nanjing 210039,China)
出处
《广州化工》
CAS
2018年第14期83-84,124,共3页
GuangZhou Chemical Industry
基金
2017年江苏省高等学校大学生实践创新训练计划一般项目(201710329044x)
关键词
气相色谱氮磷检测法
气相色谱质谱法
精密度
灵敏度
线性相关性
gas chromatography
nitrogen and phosphorus detection
gas chromatography-mass spectrometry
precision
sensitivity
linear correlation
