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硫氰酸盐光度法测定钼矿石样品中WO_3的不确定度评定

Uncertainty evaluation for determination of WO_3 in molybdenum ore samples by thiocyanate spectrophotometric method
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摘要 对用硫氰酸盐光度法测定钼矿石中WO_3的不确定度进行评定,根据结果计算公式建立数学模型,讨论了天平称样、样品定容、标准的系列配制、工作曲线的拟合、重复性测定等对WO_3测量结果引入的不确定度分量,并评估了WO_3标准不确定度和扩展不确定度。 The uncertainty of the determination of WO3 in molybdenum ore samples by thiocyanate spectrophotometric method was evaluated,and a mathematical model was established according to the formula of the results. The uncertainty components of WO3 measurement results,such as balance measurement,sample volume determination,standard series preparation,work curve fitting and repeatability measurement,are discussed. And the standard uncertainty and extended uncertainty of WO3 are evaluated.
作者 王攀峰 邰文亮 Wang Pan-feng;Tai Wen-liang(No.203 Research Institute of Nuclear Industry,Shanxi Xianyang 712000)
出处 《江西化工》 2018年第3期64-66,共3页 Jiangxi Chemical Industry
关键词 光度法 钼矿石 WO3 不确定度评定 spectrophotometric method molybdenum ore WO3 uncertainty evaluation
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