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萘二酰亚胺取代的2,4-二氯肉桂酸乙酯的合成及生物活性 被引量:1

Synthesis and Biological Activity of Naphthalene Diimide Substituted Ethyl 2,4-Dichlorocinnamate
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摘要 2-(2-羟基乙基)-1H-苯并[哒]异喹啉-1,3(2H)-二酮与2,4-二氯肉桂酰氯反应,得到了相应的肉桂酸酯类化合物3-(2,4-二氯苯基)丙烯酸-2-(1,3-二氧代-1H-苯并[哒]异喹啉-2(3H)-基)乙酯(化合物Ⅰ),其化学结构经~1H NMR和^(13)C NMR确证。室内活性实验结果表明,在质量浓度为20 mg/L时,化合物Ⅰ对小麦发芽促进率最大,达到38.8%。在质量浓度为30 mg/L时,其对小麦主根、侧根根长,茎高的促进率最大,分别为17.0%、13.0%、20.5%,优于对照药剂胺鲜酯。在质量浓度为100 mg/L时,其对小麦纹枯病菌的抑制率为93.0%。 According to active group splicing method, 2-(2-hydroxyethyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione was reacted with 2,4-dichlorocinnamoyl chloride to give naphthalene diimide substituted ester compound I. The structure of the target compound was confirmed by 1H NMR and 13C NMR. The indoor rooting sprouting experiment and bactericidal activity experiment showed that at the concentration of 20 mg/L, the germination promotion rate of compound I reached 38.8%. At the concentration of 30 mg/L, the promotion rates of compound I on the main root length, lateral root length and stem height of wheat were 17.0%, 13.0%, 20.5%, respectively. At the concentration of 100 mg/L, the inhibition rate against R. cerealis reached 93.0%.
作者 田朝瑜 许良忠 Tian Zhao-yu;Xu Liang-zhong*(College of Chemistry and Molecular Engineering,Qingdao University of Science and Technology,Shandong Qingdao 266042,China)
出处 《现代农药》 CAS 2018年第6期6-9,共4页 MODERN AGROCHEMICALS
关键词 萘二酰亚胺 二氯肉桂酸酯 合成 植物生长调节活性 抑菌活性 naphthalene diimide dichlorocinnamate synthesis plant growth-regulating activity bactericidal activity
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