摘要
The title compound 3-(difluoromethyl)-1-methyl-N-((2-(trifluoromethyl)phenyl)-carbamoyl)-1 H-pyrazole-4-carboxamide(C14 H11 F5 N4 O2) was synthesized, and its structure was confirmed by 1 H NMR, H RMS and X-ray diffraction. It crystallizes in monoclinic system, space group P21/n with a = 6.994(3), b = 13.860(6), c = 15.308(7) ?, β = 97.632(6)°, V = 1470.8(11) ?3,Z = 4, the final R = 0.0692 and wR = 0.2108 for 3989 observed reflections with Ⅰ > 2σ(Ⅰ). The preliminary biological test shows that the title compound has moderate fungicidal activities against Pseudomonas syringae.
基金
funded by the Public Science&Technology Project of Zhejiang Province(No.2017C32011)
Mid-Youth Academic Team of Zhejiang Shuren University
Natural Science Foundation of Zhejiang Province(No.LY19C140002)