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GC-MS法分析多蕊商陆挥发油中的化学成分 被引量:3

Analysis of essential oil from Phytolacca polyandra by GC-MS
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摘要 目的:分析多蕊商陆挥发油的化学成分,为其进一步研究提供实验依据。方法:采用溶剂回流法提取多蕊商陆中的挥发油,并用气相色谱-质谱技术测定分析。结果:通过计算机检索,鉴定了其中的28个化合物,占挥发油总量的95.97%。其中4-羟基-4-甲基-2-戊酮(16.78%)、棕榈酸(16.59%)、亚麻油酸(10.38%)、乙酸正二十八烷醇酯(10.28%)、硬脂酸(8.21%)、反油酸(8.19%)、柠檬酸三乙酯(7.17%)、1-萘氨基苯(5.03%)等化合物含量较高。结论:多蕊商陆挥发油由多种化合物组成,其中以脂肪酸、酯、酮、醇、芳香烃类为主。 Objective To analyze the chemical constituents of essential oil from Phytolacca polyandra.Methods The essential oil were extracted by solvent refluxing extraction and their chemical compositions were analyzed by gas chromatography-mass spectrometry(GC-MS).Results 28 constituents were identifie, total of which occupied 95.97 % of the essential oil. The major constituents were 4-Hydroxy-4-methyl-2-pentanon(16.78%), palmitic acid(16.59%), linolic acid(10.38%), n-Octacosanol acetate(10.28%), stearic acid(8.21%), elaidinic acid(8.19%), triethyl citrate(7.17%), n-Phenyl-1-naphthylamine(5.03%).Conclusion Phytolacca polyandra contains a variety of compounds mainly with fatty acids, esters, ketones, alcohols and aromatic hydrocarbons.
作者 邱开雄 谭建林 谢惠定 李玉鹏 杨绍雄 陈维金 陈丽君 QIU Kaixiong;TAN Jianlin;XIE Huiding;LI Yupeng;YANG Shaoxiong;CHEN Weijin;CHEN Lijun(School of Pharmaceutical Science and Yunnan Key Laboratory of Pharmacology for Natural Products,Kunming Medical University,Kunming 650500,China;Yunnan Product Quality Supervision and Inspection Institute,Kunming 650223,China)
出处 《中国民族民间医药》 2019年第22期55-57,共3页 Chinese Journal of Ethnomedicine and Ethnopharmacy
基金 云南省科技厅应用基础研究项目[No.2017FE468(-138)] 云南省教育厅科学研究基金指导项目(No.2017ZDX160)
关键词 多蕊商陆 挥发油 气相色谱-质谱联用法 化学成分 Phytolacca Polyandra Essential Oil Gas Chromatography-mass Spectrometry Chemical Constituents
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