摘要
化妆品中非法添加禁用物质如抗生素、抗组胺成分、激素、染料、塑化剂等,严重危害消费者的健康。由于化妆品种类繁多,基质较为复杂,合适的前处理及检测技术是有效鉴别各种非法添加物的关键。本文介绍了化妆品的提取方法,如超声萃取、震荡萃取、基质固相分散萃取以及分散液液微萃取法,对化妆品的净化手段如固相萃取技术、QuEChERS等进行阐述,归纳了化妆品非法添加物的测定方法,包括毛细管电泳色谱,气相色谱与质谱联用,液相色谱,液相色谱与质谱、飞行时间质谱、静电场轨道阱质谱等的联用,并对未来化妆品中非法添加物的分析技术作了展望。
Substances illegally added such as antibiotics, antihistamines, hormones, dyes and plasticizers in cosmetics seriously endanger the health of consumers. Due to the wide variety of cosmetics and complex matrix, appropriate pretreatments and detection technologies are the key to effectively identify various substances illegally added. This paper introduced the extraction methods of cosmetics such as ultrasonic extraction, shaking extraction, matrix solid-phase dispersion extraction and dispersion liquid-liquid microextraction.The paper expounded the purification methods of cosmetics such as solid-phase extraction technology and QuEChERS, and summarized the determination methods of substances illegally added in cosmetics, including capillary electrophoresis chromatography, gas chromatography,the combination of gas chromatography and mass spectrometry, liquid chromatography, and the combination of liquid chromatography,mass spectrometry, time of flight mass spectrometry and electrostatic field orbital trap mass spectrometry. Finally, the prospect of the determination technologies of substances illegally added in cosmetics was presented.
作者
陆奕娜
段建发
陈建伟
林文
吕坚羚
LU Yi-Na;DUAN Jian-Fa;CHEN Jian-Wei;LIN-Wen;LYU Jian-Ling(Shantou Customs,Shantou 515031)
出处
《中国口岸科学技术》
2022年第4期20-25,共6页
China Port Science and Technology
基金
汕头海关科研计划项目(2020STK005)。
关键词
化妆品
非法添加物
提取
净化
测定
cosmetics
substances illegally added
extraction
purification
determination
