摘要
利用相转移催化剂催化合成乙酸乙酯 ,最佳反应条件如下 :催化剂用量 0 5g/0 .1mol乙酸 ,醇酸比 2∶1,反应时间 40min ,收率 97 81%。实验证明 ,相转移催化对该酯化反应是高效 。
Use of CTMAB as phase transfer catalyst on the esterification of ethyl acetate was studied.The optimized donditions are as following:the weight of catalyst is 0.5g/0.1mol ethanol,the mole ratio of alchol to acid is 2∶1 and the reaction time is 0.6h.The chemical yield was 97.81b%.Experiment results showed that phase transfer catalyst(CTMAB) is a highly active catalyst for this reaction.It is an inexpensive very practical method.
出处
《化学工程师》
CAS
2002年第6期12-13,共2页
Chemical Engineer
