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比色法测定消癌平注射液中总酚酸的含量 被引量:38

Determination of total phenolic acid in Xiaoaiping injection by Colorimetry
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摘要 目的 建立消癌平注射液中总酚酸的含量测定方法。方法 以绿原酸为对照品 ,比色法测定。结果 绿原酸回归方程为A =35 8.1 4×C - 5 .3879(r=0 .9993,n =9)。在 2 0 .5~ 32 8μg范围内呈线性关系 ,平均回收率为 1 0 0 .4 8% ,RSD =1 .70 %。结论 所用方法简便、准确、快速 。 OBJECTIVE To establish a method for the determination of total phenolic acid in Xiaoaiping injection.METHODS The total phenolic acid was determined with the chlorogenic acid as a control standard by colorimetry.RESULTS A linear relationship of chlorogenic acid was good at the range of 20.5 μg to 328 μg, The average recovery of chlorogenic acid was 100.48% with RSD =1.70%.CONCLUSION The method is simple,accurate and reliable for the determination of total phenolic acid in Xiaoaiping injection.
出处 《华西药学杂志》 CAS CSCD 2003年第3期220-222,共3页 West China Journal of Pharmaceutical Sciences
关键词 消癌平注射液 中药制剂 总酚酸 含量测定 比色法 Xiaoaiping injection Determination Total phenolic acid Chlorogenic acid Colorimetry
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  • 1刘瑞玲 李维嘉 等.丹参及其注射液中水溶性总酚的测定[J].药物分析杂志,1983,3(3):163-165.
  • 2李敏 王胜春 等.五灵丸中丹参总酚性成分的含量测定[J].中成药,1990,12(1):12-12.

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