摘要
The internal friction behavior of Al green power compact duxing the sintering process was studied as a function of temperature. The internal friction measurements were performed from room temperature to 600 °C. Two typical internal friction peaks were detected corresponding to heating and cooling processes, respectively. The heating peak corresponds to a recrystallization process of deformed Al particles, which is influenced by many extrinsic parameters, such as measuring frequency, strain amplitude, heating rate, power particle size and compacting pressure. However, the intrinsic nature of the peak is originated from the micro-sliding of the weak-bonding interfaces between Al particles and increased dislocation density induced in compressing. The cooling peak with the activation energy of (1.64±0.06) eV is associated with the grain boundary relaxation, which can be interpreted as the viscous sliding of grain boundaries. The similar phenomena are also found in the Mg green powder compact.
在室温至600℃之间,研究铝粉末压坯在烧结过程中的内耗行为,其在升温和降温过程各出现一个典型的内耗峰。升温峰具有测量频率、应变振幅、升温速率依赖性,同时,随铝颗粒粒径、压坯成型压力的不同而变化。分析认为升温峰与形变铝颗粒的再结晶过程有关,但该峰产生的本征原因是形变铝颗粒之间弱结合界面的微观滑移,同时还与成型过程中位错密度的增加有关。降温峰与铝晶界的粘滞性滑移有关,属于晶界弛豫峰,其激活能为(1.64±0.06)e V。此外,镁粉末压坯具有与铝粉末压坯相似的内耗现象。
基金
Project(51301150)supported by the National Natural Science Foundation of China
Project(2013KJXX-11)supported by the Special Program of Youth New-star of Science and Technology of Shaanxi Province,China
Project(Physics-2012SXTS05)supported by the High-level University Construction Special Program of Shaanxi Province,China
