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Electrodeposition and characterization of nanocrystalline Fe-Ni-Cr alloy coatings synthesized via pulse current method 被引量:5
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作者 Ebrahim YOUSEFI ahmad irannejad Shahriar SHARAFI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第12期2591-2603,共13页
The nanocrystalline Fe-Ni-Cr coatings were electrodeposited by using the pulse current technique.The SEM results showed that the coatings had a mixed morphology of small nodules and fine cauliflower structures at low ... The nanocrystalline Fe-Ni-Cr coatings were electrodeposited by using the pulse current technique.The SEM results showed that the coatings had a mixed morphology of small nodules and fine cauliflower structures at low current densities.Also,the Cr content was increased at expense of Fe and Ni contents at high current densities.XRD patterns confirmed that the pulse current density had a positive effect on the grain refinement.The results of vibrating sample magnetometer(VSM)measurements demonstrated that by increasing the current density,the saturation magnetization was decreased and the coercivity was increased due to the enhancement of Cr content and the reduction of the grain size.The friction coefficient and wear rate values were decreased by increasing the pulse current density.Also,both the adhesive and abrasive wear mechanisms were observed on the worn surfaces.The abrasive grooves and the amount of wear debris were decreased by increasing the pulse current density. 展开更多
关键词 pulse electrodeposition current density nanocrystalline Fe-Ni-Cr coatings magnetic behavior tribological properties
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Microstructure,tribological behavior and magnetic properties of Fe−Ni−TiO_(2) composite coatings synthesized via pulse frequency variation 被引量:3
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作者 Ebrahim YOUSEFI Shahriar SHARAFI ahmad irannejad 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第12期3800-3813,共14页
The Fe−Ni−TiO_(2) nanocomposite coatings were electrodeposited by pulse frequency variation.The results showed that the nanocomposite with a very dense coating surface and a nanocrystalline structure was produced at h... The Fe−Ni−TiO_(2) nanocomposite coatings were electrodeposited by pulse frequency variation.The results showed that the nanocomposite with a very dense coating surface and a nanocrystalline structure was produced at higher frequencies.By increasing the pulse frequency from 10 to 500 Hz,the iron and TiO_(2) nanoparticles contents were increased in expense of nickel content.XRD patterns showed that by increasing the frequency to 500 Hz,an enhancement of BCC phase was observed and the grain size of deposits was reduced to 35 nm.The microhardness and the surface roughness were increased to 647 HV and 125 nm at 500 Hz due to the grain size reduction and higher incorporation of TiO_(2) nanoparticles into the Fe−Ni matrix(5.13 wt.%).Moreover,the friction coefficient and wear rate values were decreased by increasing the pulse frequency;while the saturation magnetization and coercivity values of the composite deposits were increased. 展开更多
关键词 Fe−Ni alloy coatings ELECTRODEPOSITION pulse frequency tribomechanical properties magnetic behaviors
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Applying the Protective Mn-Co-La_(2)O_(3)Coating on Crofer 22 APU Ferritic Stainless Steel Used as Solid Oxide Fuel Cell Interconnects
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作者 Farhad Mohsenifar Hadi Ebrahimifar ahmad irannejad 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2024年第5期872-888,共17页
This research studies the effect of Mn-Co-La_(2)O_(3) coating synthesized by the electrodeposition method on the oxidation resistance and electrical conductivity of the Crofer 22 APU stainless steel interconnect plate... This research studies the effect of Mn-Co-La_(2)O_(3) coating synthesized by the electrodeposition method on the oxidation resistance and electrical conductivity of the Crofer 22 APU stainless steel interconnect plates in solid oxide fuel cells.The test samples were characterized by a field emission scanning electron microscope(FESEM)equipped with energy dispersive spectroscopy(EDS),X-ray diffraction(XRD),and X-ray photoelectron spectroscopy(XPS).The oxidation kinetics of the coated and uncoated samples were studied by tracking their weight changes over time at 800°C,showing that the oxidation mechanism for all samples follows the parabolic law.Lower oxidation rate constant(k_(p))values of the coated sample compared with that of the uncoated one indicated a reduction in the oxidation rate of the steel substrate in the presence of the Mn-Co-La_(2)O_(3) coating.The examination of the cross-section of different samples after the isothermal oxidation for 500 h at 800°C exhibited that applying the composite coating leads to a decrease in the thickness of the chromia layer formed on the steel surface.Furthermore,under these conditions,the area-specific resistance(ASR)of the coated sample(13.11 mΩcm^(2))is significantly lower than that of the uncoated one(41.45 mΩcm^(2)). 展开更多
关键词 Area specific resistance Oxidation Fuel cell Composite coating
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