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超声辅助酶法降解枳实果胶及其衍生物抗氧化性能
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作者 钱伟 阳斌 +2 位作者 邵博 万力 周军 《日用化学工业(中英文)》 CAS 北大核心 2024年第8期947-955,共9页
采用超声辅助酶法对枳实果胶进行降解,获得枳实果胶降解衍生物。以抗氧化活性为指标,考察了超声预处理时间、酶种类、酶添加量等因素对枳实果胶降解衍生物抗氧化活性的影响。利用滴定法、凝胶色谱法和红外光谱等技术分析了枳实果胶降解... 采用超声辅助酶法对枳实果胶进行降解,获得枳实果胶降解衍生物。以抗氧化活性为指标,考察了超声预处理时间、酶种类、酶添加量等因素对枳实果胶降解衍生物抗氧化活性的影响。利用滴定法、凝胶色谱法和红外光谱等技术分析了枳实果胶降解衍生物中半乳糖醛酸含量、分子量分布以及结构特性,以验证果胶降解衍生物抗氧化构效关系。结果表明:当果胶酶作为降解酶,酶用量为6000 U/g,超声预处理时间为20 min时,制备的枳实果胶降解衍生物的抗氧化活性最佳,此条件下其质量浓度为3 mg/mL时,对DPPH自由基的清除率为62.94%,对ABTS自由基的清除率为52.67%,还原能力为0.9627,与未降解的枳实果胶相比,抗氧化活性显著提高。枳实果胶降解衍生物中半乳糖醛酸含量随降解工艺的不同存在明显差异,且半乳糖醛酸含量与抗氧化活性呈正相关。此外,枳实果胶降解衍生物分子量更低,且甲氧基含量也明显降低,但降解过程并没有改变果胶的吡喃糖结构。研究结果为枳实果胶的高值化利用提供理论依据和参考。 展开更多
关键词 枳实果胶 超声辅助酶法 降解衍生物 抗氧化活性 构效分析
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Primary parenchymal squamous cell carcinoma of the kidney:A case report
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作者 Zhi-Hui Zheng bo shao +4 位作者 Chao-Min Xu Ke Wang Jia-Zhu Wen Li-Kang Luo Jia-Cheng Guan 《World Journal of Clinical Cases》 SCIE 2025年第4期34-40,共7页
BACKGROUND Primary squamous cell carcinoma(SCC)of the renal parenchyma is extremely rare,with only nine cases reported.CASE SUMMARY This study reports a 51-year-old man with primary SCC of the renal parenchyma.The pat... BACKGROUND Primary squamous cell carcinoma(SCC)of the renal parenchyma is extremely rare,with only nine cases reported.CASE SUMMARY This study reports a 51-year-old man with primary SCC of the renal parenchyma.The patient was admitted with recurrent dull pain and discomfort in the right lumbar region,which had worsened over 2 weeks,accompanied by painful gross hematuria.SCC antigen(SCCA)levels were elevated,and imaging revealed a renal mass with associated calculi.The patient underwent laparoscopic unilateral nephrectomy and lymph node dissection.Postoperative pathology confirmed highly differentiated SCC with necrosis in the right renal parenchyma,with negative renal pelvis and ureter.The pathological stage was Pt3aN1M0.Four months after surgery,the tumor recurred with involvement of the liver,right psoas major muscle,and inferior vena cava.The patient refused chemotherapy and succumbed to the disease 6 months postoperatively due to disease progression.CONCLUSION We report a case of primary SCC of the renal parenchyma,a rare renal malignancy.The clinical symptoms,laboratory tests,and imaging findings are nonspecific,making accurate and timely diagnosis challenging.According to the literature,for patients with renal calculi accompanied by a renal mass,elevated serum SCCA levels,and magnetic resonance imaging showing cystic or cystic-solid masses within the kidney with pseudocapsules and heterogeneous mild enhancement,the possibility of this disease should be considered. 展开更多
关键词 Renal tumor Renal parenchyma Squamous cell carcinoma Renal calculi Computed tomography Case report
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Biodegradable interference distraction implant:a promising replacement for conventional implant in patients with insufficient alveolar bone height
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作者 Yongfeng Li Tao Li +8 位作者 bo shao Yingying Sun Yuan Gao Yongqiang Zhang Qi Gao Shuning Shen Qiang Niu Mingming Shen Liang Kong 《医用生物力学》 EI CAS CSCD 北大核心 2013年第S1期113-114,共2页
Background Dental implants have been widely used in the last few decades.However,patients with insufficient bone height need reconstructive surgeries before implant insertion.Distraction implant(Dl)has been invented t... Background Dental implants have been widely used in the last few decades.However,patients with insufficient bone height need reconstructive surgeries before implant insertion.Distraction implant(Dl)has been invented to simplify the treatment procedure,but the shortcomings of Dl have limited its clinical use.We introduced biodegradable polyester to a novel Dl,called biodegradable interference distraction implant(BIDI).The purpose of this study was to assess the radiological,histological,and biomechanical properties of BIDI in animal models.Methods BIDIs were manufactured and inserted into the atrophied mandibles of 6 dogs. 展开更多
关键词 IMPLANT DISTRACTION ALVEOLAR BIODEGRADABLE radiological insufficient REPLACEMENT polyester SHORTCOMINGS simplify
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Preliminary results on a near-real-time rock slope damage monitoring system based on relative velocity changes following the September 5,2022 M_(S) 6.8 Luding,China earthquake 被引量:1
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作者 Fan Xie Chen Liang +5 位作者 Shigui Dai bo shao Huibao Huang Jinhui Ouyang Li Li Eric Larose 《Earthquake Research Advances》 CSCD 2023年第1期31-36,共6页
Relative seismic velocity change(dv/v)is important for monitoring changes in subsurface material properties and evaluating earthquake-induced rock slope damage in a geological disaster-prone region.In this paper,we pr... Relative seismic velocity change(dv/v)is important for monitoring changes in subsurface material properties and evaluating earthquake-induced rock slope damage in a geological disaster-prone region.In this paper,we present a rapid damage assessment on three slow-moving rock slopes by measuring dv/v decrease caused by the 2022 M_(S) 6.8 Luding earthquake in Southwest China.By applying the stretching method to the cross-correlated seismic wavefields between sensors installed on each slope,we obtain earthquake-induced dv/v decreases of~2.1%,~0.5%,and~0.2%on three slopes at distances ranging from~86 to~370 km to the epicenter,respectively.Moreover,based on seismic data recorded by 16 sensors deployed on the rock slope at a distance of~370 km away from the epicenter,a localized dv/v decease region was observed at the crest of the slope by calculating the spatial dv/v images before and after the earthquake.We also derive an empirical in situ stress sensitivity of -7.29×10^(-8)/Pa by relating the dv/v change to the measured peak dynamic stresses.Our results indicate that a rapid dv/v assessment not only can help facilitate on-site emergency response to earthquakeinduced secondary geological disasters but also can provide a better understanding of the subsurface geological risks under diverse seismic loadings. 展开更多
关键词 Relative velocity change Rock slope damage Luding earthquake Space-time evolution
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Effect of clad ratio on interfacial microstructure and properties of cladding billets via direct-chill casting process 被引量:4
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作者 Hai-tao ZHANG Xing HAN +3 位作者 Dong-tao WANG bo shao Ke QIN Jian-zhong CUI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2018年第5期998-1006,共9页
Numerical simulation and experiments were introduced to develop AA4045/AA3003 cladding billets with different clad-ratios. The temperature fields, microstructures and mechanical properties near interface were investig... Numerical simulation and experiments were introduced to develop AA4045/AA3003 cladding billets with different clad-ratios. The temperature fields, microstructures and mechanical properties near interface were investigated in detail. The results show that cladding billets with different clad-ratios were fabricated successfully. Si and Mn elements diffused across the bonding interface and formed diffusion layer. With the increase of clad-layer thickness, the interfacial region transforms from semisolid-solid state to liquid-solid state and the diffusion layer increased from 10 to 25 μm. The hardness at interface is higher than that of AA3003 side but lower than that of the other side. The bonding strength increased with the clad-layer thickness, attributing to solution strengthening due to elements diffusion. The cladding billets were extruded into clad pipe by indirect extrusion process after homogenization. The clad pipe remained the interfacial characteristics of as-cast cladding billet and the heredity of clad-ratio during deformation was testified. 展开更多
关键词 cladding billet clad ratio temperature field interfacial microstzucture diffusion layer bonding strength
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Application of Benchmark Dose (BMD) in Estimating Biological Exposure Limit (BEL) to Cadmium 被引量:3
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作者 bo shao TAI-YI JIN +2 位作者 XUN-WEI WU QING-HU KONG TING-TING YE 《Biomedical and Environmental Sciences》 SCIE CAS CSCD 2007年第6期460-464,共5页
Objective To estimate the biological exposure limit (BEL) using benchmark dose (BMD) based on two sets of data from occupational epidemiology. Methods Cadmium-exposed workers were selected from a cadmium smelting ... Objective To estimate the biological exposure limit (BEL) using benchmark dose (BMD) based on two sets of data from occupational epidemiology. Methods Cadmium-exposed workers were selected from a cadmium smelting factory and a zinc product factory. Doctors, nurses or shop assistants living in the same area served as a control group. Urinary cadmium (UCd) was used as an exposure biomarker and urinary D2-microgloburin (B2M), N-acetyl-D-D-glucosaminidase (NAG) and albumin (ALB) as effect biomarkers. All urine parameters were adjusted by urinary creatinine. Software of BMDS (Version 1.3.2, EPA.U.S.A) was used to calculate BMD. Results The cut-off point (abnormal values) was determined based on the upper limit of 95% of effect biomarkers in control group. There was a significant dose response relationship between the effect biomarkers (urinary B2M, NAG9 and ALB) and exposure biomarker (UCd). BEL value was 5 μg/g creatinine for UB2M as an effect biomarker, consistent with the recommendation of WHO. BEL could be estimated by using the method of BMD. BEL value was 3 μg/g creafinine for UNAG as an effect biomarker. The more sensitive the used biomarker is, the more occupational population will be protected. Conclusion BMD can be used in estimating the biological exposure limit (BEL). UNAG is a sensitive biomarker for estimating BEL after cadmium exposure. 展开更多
关键词 Benchmark dose Biological exposure limit BIOMARKER
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Seismogenic tectonics of the Qian-Gorlos earthquake in Jilin Province,China 被引量:3
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作者 Jun Shen bo shao +4 位作者 Xiao-hui Yu Yang Yu Gao Qi Mei Deng Hanwen Zhang 《Earthquake Science》 CSCD 2016年第2期93-103,共11页
The Qian-Gorlos earthquake, which occurred in the Songliao basin in Jilin Province in 1119 AD, was the largest earthquake to occur in NE China before the 1975 Haicheng earthquake. Based on historical records and surfa... The Qian-Gorlos earthquake, which occurred in the Songliao basin in Jilin Province in 1119 AD, was the largest earthquake to occur in NE China before the 1975 Haicheng earthquake. Based on historical records and surface geological investigations, it has been suggested previously that the earthquake epicenter was in the Longkeng area. However, other workers have considered the epicenter to be in the Halamaodu area based on the landslides and faults found in this region. No seismogenic structure has yet been found in either of these two regions.We tried to detect active faults in the urban areas of Songyuan City, where the historical earthquake was probably located. One of the aims of this work was to clarify the seismogenic structure so that the seismic risk in the city could be more accurately evaluated. The area was investigated and analyzed using information from remote sensing and topographic surveys, seismic data from petroleum exploration, shallow seismic profiles, exploratory geological trenches on fault outcrops, and borehole data. The geophysical data did not reveal any evidence of faults cutting through Cretaceous or later strata under the Longkeng scarp, which has been suggested to be structural evidence of the Qian-Gorlos earthquake. The continuous fault surfaces on the back edge of terraces in theHalamaodu area stretch for [3.5 km and were probably formed by tectonic activity. However, results from shallow seismic profiles showed that the faults did not extend downward, with the corresponding deep structure being identified as a gentle kink band. A new reverse fault was found to the west of the two suggested epicenters, which presented as a curvilinear fault extending to the west, and was formed by two groups of NE- and NW-trending faults intersecting the Gudian fault. Three-dimensional seismic and shallow seismic data from petroleum exploration revealed its distinct spatial distribution and showed that the fault may cut through Late Quaternary strata. Exploration boreholes and later geomorphological studies provided further proof of this. Based on these results and analysis,the Gudian fault was confirmed as having been an active fault since the Late Quaternary, with the possibility of earthquakes of magnitude [7 in the future. The QianGorlos earthquake was most probably the result of breakage on one or two sections of this 66-km-long fault. 展开更多
关键词 Qian-Gorlos earthquake Historical earthquake Seismogenic structure
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Preparation of ZSM-5 containing vanadium and Br?nsted acid sites with high promoting of styrene oxidation using 30% H_2O_2 被引量:2
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作者 Xianfeng Liu Fu Yang +3 位作者 Shuying Gao bo shao Shijian Zhou Yan Kong 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2020年第5期1302-1310,共9页
Design and synthesis of low cost and efficacious industrial catalyst for the oxidation of styrene has been an important research project.Herein,ZSM-5 zeolite containing tetrahedral vanadium(V)and Br?nsted acid sites(V... Design and synthesis of low cost and efficacious industrial catalyst for the oxidation of styrene has been an important research project.Herein,ZSM-5 zeolite containing tetrahedral vanadium(V)and Br?nsted acid sites(V-H-ZSM-5)was prepared,and identified by characterizations such as XRD,SEM,UV–vis,NH3-TPD,H2-TPR N2-adsorption/desorption and FTIR.V-H-ZSM-5 performed extremely enhanced catalytic activity for the oxidation of styrene with 30%H2O2 at 40°C.Moreover,in-situ FTIR spectrum was used to investigate the catalytic mechanism.The results demonstrate that Br?nsted acid site could not only increase the adsorption concentration of styrene in the micropores of V-H-ZSM-5 via theπcomplex interaction between double bond of styrene and Br?nsted acid sites,but also increase the oxidation potential of H2O2.The synergetic action of tetrahedral vanadium(V)and Br?nsted acid enhanced the catalytic activity for the oxidation of styrene with 30%H2O2.Impressively,V-H-ZSM-5 performed high reusability within five runs at a low reaction temperature(40°C)for the first time. 展开更多
关键词 Selective oxidation STYRENE Bronsted acid BIFUNCTIONAL VANADIUM
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基于信息匹配的个性化推荐
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作者 邵波 李贵 +2 位作者 李征宇 韩子扬 孙平 《信息工程期刊(中英文版)》 2015年第6期182-189,共8页
个性化推荐正成为当前web推荐领域中主要研究问题之一。目前,坚于信息匹配技术在信息检索上的良好应用,针对个性化推荐,引入信息匹配概念,提出一个基于信息匹配的个性化推荐模型。通过这个模型,计算用户与每个物品之间的相关性概... 个性化推荐正成为当前web推荐领域中主要研究问题之一。目前,坚于信息匹配技术在信息检索上的良好应用,针对个性化推荐,引入信息匹配概念,提出一个基于信息匹配的个性化推荐模型。通过这个模型,计算用户与每个物品之间的相关性概率,然后根据个性化推荐的排名策略,对用户与每个物品的相关性概率值进行排序,生成用户的推荐列丧。使用MovieLens数据集,通过比较典型算法与信息匹配算法在个性化推荐上的性能,验证了基于信息匹配的个性化推荐模型的有效性。 展开更多
关键词 信息匹配 特征向量 个性化推荐 概率模型
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The investigation of DARC etch back in DRAM capacitor oxide mask opening 被引量:1
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作者 Jianqiu Hou Zengwen Hu +5 位作者 Kuowen Lai Yule Sun bo shao Chunyang Wang Xinran Liu Karson Liu 《Journal of Semiconductors》 EI CAS CSCD 2021年第7期88-92,共5页
Opening the silicon oxide mask of a capacitor in dynamic random access memory is a critical process on a capacitive coupled plasma(CCP)etch tool.Three steps,dielectric anti-reflective coating(DARC)etch back,silicon ox... Opening the silicon oxide mask of a capacitor in dynamic random access memory is a critical process on a capacitive coupled plasma(CCP)etch tool.Three steps,dielectric anti-reflective coating(DARC)etch back,silicon oxide etch and strip,are contained.To acquire good performance,such as low leakage current and high capacitance,for further fabricating capacitors,we should firstly optimize DARC etch back.We developed some experiments,focusing on etch time and chemistry,to evalu-ate the profile of a silicon oxide mask,DARC remain and critical dimension.The result shows that etch back time should be con-trolled in the range from 50 to 60 s,based on the current equipment and condition.It will make B/T ratio higher than 70%mean-while resolve the DARC remain issue.We also found that CH_(2)F_(2) flow should be~15 sccm to avoid reversed CD trend and keep in-line CD. 展开更多
关键词 dynamic random access memory(DRAM) oxide mask open of capacitor capacitive coupled plasma(CCP)etch dielectric anti-reflective coating(DARC) etch back(EB)
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Interfacial characteristics and properties of a low-clad-ratio AA4045/AA3003 cladding billet fabricated by semi-continuous casting 被引量:2
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作者 Xing Han Hai-tao Zhang +3 位作者 bo shao Lei Li Ke Qin Jian-zhong Cui 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第9期1097-1103,共7页
A low-clad-ratio AA4045/AA3003 cladding billet was fabricated using a semi-continuous casting process and was subsequently extruded indirectly into a cladding pipe. The temperature distribution near the interface was ... A low-clad-ratio AA4045/AA3003 cladding billet was fabricated using a semi-continuous casting process and was subsequently extruded indirectly into a cladding pipe. The temperature distribution near the interface was measured. The microstructures, elemental distribution, Vickers hardness around the bonding interface, and the interfacial shear strength were examined. The results showed that the interface temperature rebounded when AA4045 melt contacted the supporting layer. The two alloys bonded well, with few defects, via the diffusion of Si and Mn in the temperature range from 569℃ to 632℃. The mean shear strength of the bonding interface was 82.3 MPa, which was greater than that of AA3003(75.8 MPa), indicating that the two alloys bonded with each other metallurgically via elemental interdiffusion. Moreover, no relative slip occurred between the two alloys during the extrusion process. 展开更多
关键词 aluminum alloys metal cladding casting interdiffusion interfaces
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Active faults and seismogenic models for the Urumqi city,Xinjiang Autonomous Region, China
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作者 Yingzhen Li Yang Yu +3 位作者 Jun Shen bo shao Gao Qi Mei Deng 《Earthquake Science》 CSCD 2016年第3期173-184,共12页
We have studied the characteristics of the active faults and seismicity in the vicinity of Urumqi city, the capital of Xinjiang Autonomous Region, China, and have proposed a seismogenic model for the assessment of ear... We have studied the characteristics of the active faults and seismicity in the vicinity of Urumqi city, the capital of Xinjiang Autonomous Region, China, and have proposed a seismogenic model for the assessment of earthquake hazard in this area. Our work is based on an integrated analysis of data from investigations of active faults at the surface, deep seismic reflection soundings, seismic profiles from petroleum exploration, observations of temporal seismic stations, and the precise location of small earthquakes. We have made a comparative study of typical seismogenic structures in the frontal area of the North Tianshan Mountains, where Urumqi city is situated, and have revealed the primary features of the thrust-fold- nappe structure there. We suggest that Urumqi city is comprised two zones of seismotectonics which are inter- preted as thrust-nappe structures. The first is the thrust nappe of the North Tianshan Mountains in the west, con- sisting of the lower (root) thrust fault, middle detachment, and upper fold-uplift at the front. Faults active in the Pleistocene are present in the lower and upper parts of this structure, and the detachment in the middle spreads toward the north. In the future, M7 earthquakes may occur at the root thrust fault, while the seismic risk of frontal fold-uplift at the front will not exceed M6.5. The second structure is the western flank of the arc-like Bogda nappe in the east, which is also comprised a root thrust fault, middle detachment, and upper fold-uplift at the front, of which the nappe stretches toward the north; several active faults are also developed in it. The fault active in the Holocene is called the South Fukang fault. It is not in the urban area of Urumqi city. The other three faults are located in the urban area and were active in the late Pleistocene. In these cases, this section of the nappe structure near the city has an earthquake risk of M6.5-7, An earthquake Ms6.6, 60 km east to Urumqi city occurred along the structure in 1965. 展开更多
关键词 URUMQI Active fault Seismogenic structure THRUST NAPPE
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Boosting solar steam generation by structure enhanced energy management 被引量:13
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作者 Yida Wang Xuan Wu +3 位作者 bo shao Xiaofei Yang Gary Owens Haolan Xu 《Science Bulletin》 SCIE EI CAS CSCD 2020年第16期1380-1388,M0004,共10页
Interfacial solar-steam generation is a promising and cost-effective technology for both desalination and wastewater treatment.This process uses a photothermal evaporator to absorb sunlight and convert it into heat fo... Interfacial solar-steam generation is a promising and cost-effective technology for both desalination and wastewater treatment.This process uses a photothermal evaporator to absorb sunlight and convert it into heat for water evaporation.However solar-steam generation can be somewhat inefficient due to energy losses via conduction,convection and radiation.Thus,efficient energy management is crucial for optimizing the performance of solar-steam generation.Here,via elaborate design of the configuration of photothermal materials,as well as warm and cold evaporation surfaces,performance in solar evaporation was significantly enhanced.This was achieved via a simultaneous reduction in energy loss with a net increase in energy gain from the environment,and recycling of the latent heat released from vapor condensation,diffusive reflectance,thermal radiation and convection from the evaporation surface.Overall,by using the new strategy,an evaporation rate of 2.94 kg m^-2 h^-1,with a corresponding energy efficiency of solar-steam generation beyond theoretical limit was achieved. 展开更多
关键词 Solar-steam generation PHOTOTHERMAL Energy management Latent heat recycling Reduced graphene oxide DESALINATION
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Estimation method of SBAS dual-frequency range error integrity parameter 被引量:7
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作者 bo shao Qun Ding Xianbing Wu 《Satellite Navigation》 2020年第1期93-100,共8页
The development of a dual-frequency multi-constellation satellite-based augmentation system(DFMC SBAS)is in progress worldwide.The broadcasted dual-frequency range error(DFRE)integrity parameter reflects the effects o... The development of a dual-frequency multi-constellation satellite-based augmentation system(DFMC SBAS)is in progress worldwide.The broadcasted dual-frequency range error(DFRE)integrity parameter reflects the effects of satellite ephemeris and clock corrections.A user uses the DFRE to calculate the protection level and then determines whether the DFMC SBAS service satisfies the requirements of the current flight phase.However,the calculation of the DFRE has not been reported.Herein,a DFRE estimation method is proposed based on the projection method.Using the ephemeris-clock covariance matrix of each satellite,the maximal projection direction was solved,and the projection of the covariance matrix on this direction was used as the DFRE to form an envelope for the maximal corrected error.Results show that the DFRE can form an envelope of the maximal corrected error with a set probability,and the integrity performance in the user segment satisfies the Category I precision approach requirement. 展开更多
关键词 Satellite-based augmentation system Dual-frequency multi-constellation Dual-frequency range error INTEGRITY
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论淮阳泥泥狗的传承与创新
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作者 邵波 《民艺》 2018年第S1期145-147,共3页
一、维系泥泥狗的产生、存在和发展的文化历史因素和社会条件民间彩绘泥塑艺术泥泥狗特产于河南淮阳。淮阳地处豫东平原,古称宛丘、陈。《左传》记载为'太昊之墟'。平粮台遗址被最新的考古发掘证实其最早为六千多年前的大汶口... 一、维系泥泥狗的产生、存在和发展的文化历史因素和社会条件民间彩绘泥塑艺术泥泥狗特产于河南淮阳。淮阳地处豫东平原,古称宛丘、陈。《左传》记载为'太昊之墟'。平粮台遗址被最新的考古发掘证实其最早为六千多年前的大汶口文化遗址和4500年前的龙山文化古城。 展开更多
关键词 淮阳泥泥狗 太昊伏羲氏 人祖猴
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