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Effect of mixing temperature on microstructure of an Al-Si alloy prepared by controlled diffusion solidification
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作者 Han Xue Ti-jun Chen +3 位作者 Xue-zheng Zhang guang-li bi Ying Ma Ren-guo Guan 《China Foundry》 SCIE CAS CSCD 2023年第3期241-252,共12页
The effects of mixing temperature,i.e.,the temperatures of two precursor melts(pure Al and Al-12Si),on the temperature and solute fields of resultant mixture,the nucleation and growth,and the size and morphology of pr... The effects of mixing temperature,i.e.,the temperatures of two precursor melts(pure Al and Al-12Si),on the temperature and solute fields of resultant mixture,the nucleation and growth,and the size and morphology of primary grains during controlled diffusion solidification(CDS) of Al-8Si alloy were investigated by using simulation and calculation.The results indicate that a lower mixing temperature is helpful for achieving more supercooled microscale Al-rich pockets in the mixture,and increasing the width and supercooling degree of supercooling zone in the Al-rich pockets,and thus,the nucleation rate.The nuclei grow up in nondendritic mode,resulting in spheroidal,at least,nondendritic grains.In a successful CDS,the superheat degrees of the two precursor melts should be limited within several degrees,and it is not necessary to extra stipulate the superheat degree of target alloy melt(Al-8Si) when the requirement about Gibbs energies of the three melts is matched.Subsequent observation on casting microstructures shows that the employed simulation and calculation processes are reasonable and the achieved results are reliable. 展开更多
关键词 controlled diffusion solidification Al-Si alloy nucleation and growth SUPERCOOLING nondendritic grains
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熔体处理温度及保温参数对A356铝合金半固态浆料水淬组织的影响(英文) 被引量:6
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作者 李明 李元东 +3 位作者 毕广利 黄晓锋 陈体军 马颖 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2018年第3期393-403,共11页
采用自孕育法制备A356铝合金半固态浆料,研究熔体处理温度及保温参数对A356铝合金半固态浆料水淬组织的影响,并分析剩余液相的二次凝固行为。结果表明:熔体处理温度对最终半固态组织影响较为显著。当熔体温度在680~690°C之间时,可... 采用自孕育法制备A356铝合金半固态浆料,研究熔体处理温度及保温参数对A356铝合金半固态浆料水淬组织的影响,并分析剩余液相的二次凝固行为。结果表明:熔体处理温度对最终半固态组织影响较为显著。当熔体温度在680~690°C之间时,可以制备出适合流变成形的半固态浆料。在等温保温过程中初生颗粒的生长速率符合D_t^3-D_0~3=Kt动力学方程,且当保温温度为600°C时初生颗粒的粗化速率最快。此外,等温保温时间对二次凝固组织的影响较明显。保温3 min时浆料水淬组织中的二次颗粒最为细小、圆整。随保温温度的升高,二次颗粒数目逐渐增多。因此,共晶反应被限制在很小的晶间区域内,使最终凝固的共晶组织排列较为紧密。 展开更多
关键词 铝合金 半固态 自孕育法 二次凝固 初生颗粒 共晶组织
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固溶和冷却处理对Mg-Dy-Ni合金中长程堆垛有序(LPSO)相形貌及析出硬化行为的影响(英文) 被引量:4
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作者 袁利桃 毕广利 +4 位作者 李元东 姜静 韩宇翔 房大庆 马颖 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2017年第11期2381-2389,共9页
研究了固溶和冷却处理对Mg-2Dy-0.5Ni(摩尔分数,%)合金中的长程堆垛有序(LPSO)相形貌及析出硬化行为的影响。铸态合金组织主要包括α-Mg相、分布在枝晶间具有LPSO结构的竹尖状Mg_(12)DyNi相和少量立方体状的Dy相。在565℃固溶处理12 h... 研究了固溶和冷却处理对Mg-2Dy-0.5Ni(摩尔分数,%)合金中的长程堆垛有序(LPSO)相形貌及析出硬化行为的影响。铸态合金组织主要包括α-Mg相、分布在枝晶间具有LPSO结构的竹尖状Mg_(12)DyNi相和少量立方体状的Dy相。在565℃固溶处理12 h及随后不同的冷却过程中,点状、块状、细薄片状和棒状的LPSO相分别在基体中析出。在连续冷却(空冷和炉冷)的条件下,细薄片状的LPSO相逐渐在晶粒内部析出;随着冷却时间的延长,其体积分数亦增加,且块状的LPSO相发生粗化。在不连续冷却(炉冷到415℃+空冷和炉冷到265℃+空冷)条件下,点状LPSO相生长成棒状相,降低了合金的冷却硬化作用。 展开更多
关键词 Mg.Dy.Ni合金 LPSO相 显微组织 析出硬化
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Effect of Zn, Cu and Ni addition on microstructure and mechanical properties of ascast Mg-Dy alloys 被引量:3
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作者 guang-li bi Xiao-mei Luo +5 位作者 Jing Jiang Yong-gang Zhang Jian-ji Xu Jie-ming Chen Yuan-dong Li Ying Ma 《China Foundry》 SCIE 2016年第1期54-58,共5页
This paper presents some research information on the effects of Zn, Cu and Ni on the microstructure and mechanical properties of as-cast Mg-2Dy(at.%) alloys. The Mg-2Dy alloy is composed of α-Mg and Mg24Dy5 phases. W... This paper presents some research information on the effects of Zn, Cu and Ni on the microstructure and mechanical properties of as-cast Mg-2Dy(at.%) alloys. The Mg-2Dy alloy is composed of α-Mg and Mg24Dy5 phases. With the addition of 0.5at.%Zn, 0.5at.%Cu and 0.5at.%Ni, respectively, besides α-Mg, the long period stacking order(LPSO) phases containing Zn, Cu, and Ni precipitated in the α-Mg interdentritic boundary. The addition of Ni effectively refined the dendrite arm spacing. The as-cast Mg-2Dy-0.5Ni alloy exhibited the best tensile strengths and elongation. The better mechanical properties were mainly attributed to small secondry dendrite arm spacing(SDAS) and high volume fraction of LPSO phases. 展开更多
关键词 Mg-Dy-Zn(Cu Ni) alloys LPSO phase microstructure mechanical properties
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Efficient fabrication of semisolid nondendritic Al alloy slurry with high quality 被引量:1
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作者 Zong-xu Zhang Ti-jun Chen +4 位作者 Kun Liu Han Xue Jia-chen Qi guang-li bi Ying Ma 《China Foundry》 SCIE CAS 2022年第2期117-130,共14页
Subjecting a normal mechanical vibration to a cooling slope plate,is a proposed method for preparing semisolid nondendritic slurry,named shear-vibration coupling sub-rapid solidification(SCS).Taking Al-8Si alloy as mo... Subjecting a normal mechanical vibration to a cooling slope plate,is a proposed method for preparing semisolid nondendritic slurry,named shear-vibration coupling sub-rapid solidification(SCS).Taking Al-8Si alloy as model material,the temperature field and distribution field of solid or liquid phase during SCS were simulated using COMSOL Multiphysics software to primarily choose the optimal processing parameters.Subsequently,the slurries were prepared with the parameters selected according to the simulation results and the microstructures of the slurries were experimentally investigated.Results indicate that the simulation results could provide a basis for roughly choosing the processing parameters,although the calculated solid fractions are always higher than the experimental ones.The processing parameters affect the primary grain size,shape factor and solid fraction mainly through altering the contact duration of melt on the plate,and thus affecting the cooling effect on the melt,nucleation rate,and grain dissociation and proliferation.Experiments with optimized processing parameters show that the primary grains in the slurry have an average size of about 32μm and shape factor of 1.38,and are quite uniform,even at the highest pouring rate of 2.81 kg·s^(-1),the size and shape factor are about 46μm and 1.7,respectively,which implies that the proposed SCS is a promising technology for efficient fabrication of high-quality Al slurry available for engineering applications. 展开更多
关键词 semisolid nondendritic slurry semisolid forming simulation primary grains shape factor
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Microstructural evolution and age-hardening behavior of quasicrystal-reinforced Mg-Dy-Zn alloy 被引量:2
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作者 guang-li bi Yu-Xiang Han +3 位作者 Jing Jiang Chun-Hong Jiang Yuan-Dong Li Ying Ma 《Rare Metals》 SCIE EI CAS CSCD 2019年第8期739-745,共7页
Microstructural evolution and age-hardening behavior of Mg-2 Dy-6 Zn(at%)alloy during solid-solution and aging treatment were investigated.The microstructure of as-cast alloy is composed of a-Mg,Mg3 DyZn6(Ⅰ)phase,Mg3... Microstructural evolution and age-hardening behavior of Mg-2 Dy-6 Zn(at%)alloy during solid-solution and aging treatment were investigated.The microstructure of as-cast alloy is composed of a-Mg,Mg3 DyZn6(Ⅰ)phase,Mg3 Dy2 Zn3(W)phase,Mg(Zn,Dy)phase and a small amount of Mg0.97Zn0.03 phases.After solid-solution treatment(480℃,12 h),all the I phases and most W phases dissolve into a-Mg matrix and the remainder W phases transform into Mg(Dy,Zn)phase and MgDy3 phase.During aging treatment,I phase and small amounts of W phases co-precipitate from α-Mg matrix,respectively.The alloy exhibits a peak hardness of HV 77.5 at 200 ℃ for 8 h.The excellent age-hardening behavior of alloy is mainly attributed to the co-precipitation strengthening of I and W phases. 展开更多
关键词 Mg-Dy-Zn ALLOY Microstructure I phase AGE-HARDENING BEHAVIOR
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