One factor that limits development of fundamental research on the infuence of coke microstructure on its strength is the difculty in quantifying the way that microstructure is both classifed and distributed in three d...One factor that limits development of fundamental research on the infuence of coke microstructure on its strength is the difculty in quantifying the way that microstructure is both classifed and distributed in three dimensions.To support such fundamental studies,this study evaluated a novel volumetric approach for classifying small(approx.450μm^(3))blocks of coke microstructure from 3D computed tomography scans.An automated process for classifying microstructure blocks was described.It is based on Landmark Multi-Dimensional Scaling and uses the Bhattacharyya metric and k-means clustering.The approach was evaluated using 27 coke samples across a range of coke with diferent properties and reliably identifed 6 ordered class of coke microstructure based on the distribution of voxel intensities associated with structural density.The lower class(1–2)subblocks tend to be dominated by pores and thin walls.Typically,there is an increase in wall thickness and reduced pore sizes in the higher classes.Inert features are also likely to be seen in higher classes(5–6).In general,this approach provides an efcient automated means for identifying the 3D spatial distribution of microstructure in CT scans of coke.展开更多
基金the Australian Coal Industry's Research Program(ACARP)-Grant Number C29073.
文摘One factor that limits development of fundamental research on the infuence of coke microstructure on its strength is the difculty in quantifying the way that microstructure is both classifed and distributed in three dimensions.To support such fundamental studies,this study evaluated a novel volumetric approach for classifying small(approx.450μm^(3))blocks of coke microstructure from 3D computed tomography scans.An automated process for classifying microstructure blocks was described.It is based on Landmark Multi-Dimensional Scaling and uses the Bhattacharyya metric and k-means clustering.The approach was evaluated using 27 coke samples across a range of coke with diferent properties and reliably identifed 6 ordered class of coke microstructure based on the distribution of voxel intensities associated with structural density.The lower class(1–2)subblocks tend to be dominated by pores and thin walls.Typically,there is an increase in wall thickness and reduced pore sizes in the higher classes.Inert features are also likely to be seen in higher classes(5–6).In general,this approach provides an efcient automated means for identifying the 3D spatial distribution of microstructure in CT scans of coke.