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Preparation of Ultrafine Cobalt Powder by Chemical Reduction in Aqueous Solution 被引量:1
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作者 Jin Zhang GAO Yan Chun ZHAO +6 位作者 Jian Niao TIAN Wu YANG Fei GUAN Xiao Quan LU yong jun ma Jing Guo HOU Jing Wan KANG 《Chinese Chemical Letters》 SCIE CAS CSCD 2001年第6期555-558,共4页
Nanocrystalline cobalt powders have been prepared from aqueous solution by reducing their corresponding metal salts under suitable conditions. The experimental conditions have been studied in detail. X-ray powder diff... Nanocrystalline cobalt powders have been prepared from aqueous solution by reducing their corresponding metal salts under suitable conditions. The experimental conditions have been studied in detail. X-ray powder diffraction patterns show that the cobalt powder is hexagonal crystallite. The average particle size of the ultrafine cobalt powder is 55 nm. 展开更多
关键词 NANOCRYSTALLINE cobalt powder PREPARATION
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In-situ Thin Layer Spectroelectrochemical Study of the Redox Mechanism add Intermediate for Vitamin B_2 in Aqueous Solution
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作者 yong jun ma Shi Min ZHU(Department of Chemistry, Nanjing University,Nanjing,210093) 《Chinese Chemical Letters》 SCIE CAS CSCD 1996年第9期825-828,共4页
The electrochemical reaction mechanism of Vitamin B2 on platinum electrode in acid aqueous solution has been studied by then layer cyclic voltammetry(TLCV) and thin layer spectroelectrochemistry (TLSEC).The results in... The electrochemical reaction mechanism of Vitamin B2 on platinum electrode in acid aqueous solution has been studied by then layer cyclic voltammetry(TLCV) and thin layer spectroelectrochemistry (TLSEC).The results indicate that there is a redox process of VB2 via a semiquinone radical to dihydroflavin. The radical intermediate has been detected by in-situ UVSEC method for the first time. 展开更多
关键词 THIN LAYER AQUEOUS INTERMEDIATE
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